1-(3-bromo-4-tert-butylsulfanylphenyl)-3-(3,5-dichlorophenyl)-4,4,4-trifluoro-3-sulfanyl-butan-1-one

Base Information

Chemical Name:1-(3-bromo-4-tert-butylsulfanylphenyl)-3-(3,5-dichlorophenyl)-4,4,4-trifluoro-3-sulfanyl-butan-1-one
CAS No.:1610614-78-2
Molecular Formula:C₂₀H₁₈BrCl₂F₃OS₂
Molecular Weight:546.3
Hs Code.:

Synonyms:1-(3-bromo-4-tert-butylsulfanylphenyl)-3-(3,5-dichlorophenyl)-4,4,4-trifluoro-3-sulfanyl-butan-1-one

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Chemical Property of 1-(3-bromo-4-tert-butylsulfanylphenyl)-3-(3,5-dichlorophenyl)-4,4,4-trifluoro-3-sulfanyl-butan-1-one

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Technology Process of 1-(3-bromo-4-tert-butylsulfanylphenyl)-3-(3,5-dichlorophenyl)-4,4,4-trifluoro-3-sulfanyl-butan-1-one

There total 1 articles about 1-(3-bromo-4-tert-butylsulfanylphenyl)-3-(3,5-dichlorophenyl)-4,4,4-trifluoro-3-sulfanyl-butan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1610609-40-9
(Z)-1-(3-bromo-4-tert-butylsulfanyl-phenyl)-3-(3,5-dichlorophenyl)-4,4,4-trifluoro-but-2-en-1-one

: 1610614-78-2
1-(3-bromo-4-tert-butylsulfanylphenyl)-3-(3,5-dichlorophenyl)-4,4,4-trifluoro-3-sulfanyl-butan-1-one

Guidance literature:: With triethylamine; tiolacetic acid; at 20 ℃; for 24h; Inert atmosphere;

Reference yield:

: 1610614-78-2
1-(3-bromo-4-tert-butylsulfanylphenyl)-3-(3,5-dichlorophenyl)-4,4,4-trifluoro-3-sulfanyl-butan-1-one

: 1610614-71-5
3-(3-bromo-4-tert-butylsulfanylphenyl)-5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazole

Guidance literature:: With ammonium bisulphate; potassium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 0.5h;

Reference yield:

: 1610614-78-2
1-(3-bromo-4-tert-butylsulfanylphenyl)-3-(3,5-dichlorophenyl)-4,4,4-trifluoro-3-sulfanyl-butan-1-one

: 1610614-67-9
2-[2-bromo-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]phenyl]sulfanylacetic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: ammonium bisulphate; potassium hydroxide / tetrahydrofuran; water / 0.5 h / 20 °C

2.1: aluminum (III) chloride / toluene / 5.17 h / 0 - 20 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0 °C

3.2: 0.67 h

4.1: trifluoroacetic acid / dichloromethane / 21.5 h / 20 °C

With aluminum (III) chloride; ammonium bisulphate; potassium tert-butylate; trifluoroacetic acid; potassium hydroxide; In tetrahydrofuran; dichloromethane; water; toluene;