2-bromo-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]benzenethiol

Base Information

Chemical Name:2-bromo-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]benzenethiol
CAS No.:1610614-73-7
Molecular Formula:C₁₆H₉BrCl₂F₃NS₂
Molecular Weight:487.191
Hs Code.:

Synonyms:2-bromo-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]benzenethiol

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Chemical Property of 2-bromo-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]benzenethiol

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Technology Process of 2-bromo-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]benzenethiol

There total 3 articles about 2-bromo-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]benzenethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1610614-71-5
3-(3-bromo-4-tert-butylsulfanylphenyl)-5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazole

: 1610614-73-7
2-bromo-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]benzenethiol

Guidance literature:: With aluminum (III) chloride; In toluene; at 0 - 20 ℃; for 5.16667h;

Reference yield:

: 1610614-78-2
1-(3-bromo-4-tert-butylsulfanylphenyl)-3-(3,5-dichlorophenyl)-4,4,4-trifluoro-3-sulfanyl-butan-1-one

: 1610614-73-7
2-bromo-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]benzenethiol

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium bisulphate; potassium hydroxide / tetrahydrofuran; water / 0.5 h / 20 °C

2: aluminum (III) chloride / toluene / 5.17 h / 0 - 20 °C

With aluminum (III) chloride; ammonium bisulphate; potassium hydroxide; In tetrahydrofuran; water; toluene;

Reference yield:

: 1610609-40-9
(Z)-1-(3-bromo-4-tert-butylsulfanyl-phenyl)-3-(3,5-dichlorophenyl)-4,4,4-trifluoro-but-2-en-1-one

: 1610614-73-7
2-bromo-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]benzenethiol

Guidance literature:: Multi-step reaction with 3 steps

1: tiolacetic acid; triethylamine / 24 h / 20 °C / Inert atmosphere

2: ammonium bisulphate; potassium hydroxide / tetrahydrofuran; water / 0.5 h / 20 °C

3: aluminum (III) chloride / toluene / 5.17 h / 0 - 20 °C

With aluminum (III) chloride; ammonium bisulphate; triethylamine; tiolacetic acid; potassium hydroxide; In tetrahydrofuran; water; toluene;