trans-1-(benzoylamino)-3-<<(methylsulfonyl)oxy>methyl>cyclobutane-N,N-pentamethylenecarboxamide

Base Information

Chemical Name:trans-1-(benzoylamino)-3-<<(methylsulfonyl)oxy>methyl>cyclobutane-N,N-pentamethylenecarboxamide
CAS No.:166667-10-3
Molecular Formula:C₁₉H₂₆N₂O₅S
Molecular Weight:394.492
Hs Code.:

Synonyms:trans-1-(benzoylamino)-3-<<(methylsulfonyl)oxy>methyl>cyclobutane-N,N-pentamethylenecarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-1-(benzoylamino)-3-<<(methylsulfonyl)oxy>methyl>cyclobutane-N,N-pentamethylenecarboxamide

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Technology Process of trans-1-(benzoylamino)-3-<<(methylsulfonyl)oxy>methyl>cyclobutane-N,N-pentamethylenecarboxamide

There total 1 articles about trans-1-(benzoylamino)-3-<<(methylsulfonyl)oxy>methyl>cyclobutane-N,N-pentamethylenecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 124-63-0
methanesulfonyl chloride

: 161181-57-3
trans-1-(benzoylamino)-3-(hydroxymethyl)cyclobutane-1-N,N-pentamethylenecarboxamide

: 166667-10-3
trans-1-(benzoylamino)-3-<<(methylsulfonyl)oxy>methyl>cyclobutane-N,N-pentamethylenecarboxamide

Guidance literature:: With triethylamine; In dichloromethane;

Reference yield: 70.0%

: 166667-10-3
trans-1-(benzoylamino)-3-<<(methylsulfonyl)oxy>methyl>cyclobutane-N,N-pentamethylenecarboxamide

: 184103-23-9
N-[3-Azidomethyl-1-(piperidine-1-carbonyl)-cyclobutyl]-benzamide

Guidance literature:: With N,N,N',N'-tetramethylguanidinium azide; In various solvent(s); at 80 ℃; for 2h;
DOI:10.1021/jm960390t

Reference yield:

: 166667-10-3
trans-1-(benzoylamino)-3-<<(methylsulfonyl)oxy>methyl>cyclobutane-N,N-pentamethylenecarboxamide

: 184103-71-7
1-Amino-3-(benzyloxycarbonylamino-methyl)-cyclobutanecarboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / N,N,N',N'-tetramethylguanidinium azide / various solvent(s) / 2 h / 80 °C

2: H₂ / 10percent Pd/C / ethanol / 20 h / 760 Torr / Ambient temperature

3: 97 percent / 6N aq. HCl / 20 h / 130 °C

4: 1.) aq. basic CuCO₃, 2.) MgO, 3.) 0.9 N aq. HCl, Na₂S

With hydrogenchloride; sodium sulfide; copper (II) carbonate hydroxide; N,N,N',N'-tetramethylguanidinium azide; hydrogen; magnesium oxide; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm960390t