[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid

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Chemical Name:[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid
CAS No.:936132-32-0
Molecular Formula:C₆₄H₆₇NO₁₄
Molecular Weight:1074.23
Hs Code.:

Synonyms:[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid

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Chemical Property of [2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid

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Technology Process of [2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid

There total 4 articles about [2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 936132-31-9
[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

: 936132-32-0
[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1002/ejoc.200600993

Reference yield:

: 913725-93-6
(2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-(4-methoxy-benzyloxymethyl)-tetrahydro-pyran-2-carboxylic acid

: 936132-32-0
[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / diphenyl phosphoryl azide; Et₃N / benzene / 4 h / Heating

2: 95 percent / LiOH / methanol; H₂O; tetrahydrofuran

With lithium hydroxide; diphenyl phosphoryl azide; triethylamine; In tetrahydrofuran; methanol; water; benzene; 1: Curtius rearrangement;
DOI:10.1002/ejoc.200600993

Reference yield:

: C₃₇H₄₀O₈

: 936132-32-0
[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / DDQ

2: 84 percent / diphenyl phosphoryl azide; Et₃N / benzene / 4 h / Heating

3: 95 percent / LiOH / methanol; H₂O; tetrahydrofuran

With lithium hydroxide; diphenyl phosphoryl azide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; water; benzene; 2: Curtius rearrangement;
DOI:10.1002/ejoc.200600993