[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

Base Information

Chemical Name:[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester
CAS No.:936132-31-9
Molecular Formula:C₆₅H₆₉NO₁₄
Molecular Weight:1088.26
Hs Code.:

Synonyms:[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

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Chemical Property of [2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

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Technology Process of [2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

There total 3 articles about [2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 913725-93-6
(2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-(4-methoxy-benzyloxymethyl)-tetrahydro-pyran-2-carboxylic acid

: 177213-12-6
(2R,3R,4S,5R,6R)-methyl 3,4,5-tris(benzyloxy)-tetrahydro-6-(hydroxymethyl)-2H-pyran-2-carboxylate

: 936132-31-9
[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; In benzene; for 4h; Heating;
DOI:10.1002/ejoc.200600993

Reference yield:

: 913725-93-6
(2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-(4-methoxy-benzyloxymethyl)-tetrahydro-pyran-2-carboxylic acid

: 936132-31-9
[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / NaHCO₃

2: 96 percent / DDQ

3: 84 percent / diphenyl phosphoryl azide; Et₃N / benzene / 4 h / Heating

With diphenyl phosphoryl azide; sodium hydrogencarbonate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; 3: Curtius rearrangement;
DOI:10.1002/ejoc.200600993

Reference yield:

: C₃₇H₄₀O₈

: 936132-31-9
[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / DDQ

2: 84 percent / diphenyl phosphoryl azide; Et₃N / benzene / 4 h / Heating

With diphenyl phosphoryl azide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; 2: Curtius rearrangement;
DOI:10.1002/ejoc.200600993