(2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-(4-methoxy-benzyloxymethyl)-tetrahydro-pyran-2-carboxylic acid

Base Information

• Chemical Name: (2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-(4-methoxy-benzyloxymethyl)-tetrahydro-pyran-2-carboxylic acid
• CAS No.: 913725-93-6
• Molecular Formula: C₃₆H₃₈O₈
• Molecular Weight: 598.693

Synonyms:(2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-(4-methoxy-benzyloxymethyl)-tetrahydro-pyran-2-carboxylic acid

Chemical Property of (2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-(4-methoxy-benzyloxymethyl)-tetrahydro-pyran-2-carboxylic acid

Chemical Property:

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Technology Process of (2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-(4-methoxy-benzyloxymethyl)-tetrahydro-pyran-2-carboxylic acid

There total 1 articles about (2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-(4-methoxy-benzyloxymethyl)-tetrahydro-pyran-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

[(2S,3S,4R,5R,6R)-3,4,5-Tris-benzyloxy-6-(4-methoxy-benzyloxymethyl)-tetrahydro-pyran-2-yl]-methanol → (2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-(4-methoxy-benzyloxymethyl)-tetrahydro-pyran-2-carboxylic acid (913725-93-6)

Guidance literature:

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; calcium chlorite; In phosphate buffer; acetonitrile;

DOI:10.1016/j.tetlet.2006.07.139

Reference yield: 100.0%

(2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-(4-methoxy-benzyloxymethyl)-tetrahydro-pyran-2-carboxylic acid (913725-93-6) + methyl iodide (74-88-4) → C37H40O8

Guidance literature:

With sodium hydrogencarbonate;

DOI:10.1002/ejoc.200600993

Reference yield: 94.0%

(2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-(4-methoxy-benzyloxymethyl)-tetrahydro-pyran-2-carboxylic acid (913725-93-6) + cholesterol (57-88-5) → [3,4,5-tris-benzyloxy-6-(4-methoxy-benzyloxymethyl)-tetrahydro-pyran-2-yl]-carbamic acid 17-(1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

Guidance literature:

With diphenylphosphoranyl azide; potassium carbonate; triethylamine; In benzene; for 15h; Heating;

DOI:10.1016/j.tetlet.2006.07.139

Downstream raw materials:

[(2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-(4-methoxy-benzyloxymethyl)-tetrahydro-pyran-2-yl]-carbamic acid (2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethyl ester

[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid

[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

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