Technology Process of C35H51N3O14
There total 10 articles about C35H51N3O14 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: aq. Ba(OH)2
2: 1.) sodium naphthalene
3: PDC / dimethylformamide
5: H2 / Pd/C
6: KF(H2O)2
7: TFA / CH2Cl2
8: (benzotriazol-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate, diisopropylethylamine
9: TFA / CH2Cl2
10: (benzotriazol-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate, diisopropylethylamine
With
potassium fluoride; barium dihydroxide; dipyridinium dichromate; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; sodium naphthalenide; trifluoroacetic acid;
palladium on activated charcoal;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00140a025
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 1.) sodium naphthalene
2: PDC / dimethylformamide
4: H2 / Pd/C
5: KF(H2O)2
6: TFA / CH2Cl2
7: (benzotriazol-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate, diisopropylethylamine
8: TFA / CH2Cl2
9: (benzotriazol-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate, diisopropylethylamine
With
potassium fluoride; dipyridinium dichromate; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; sodium naphthalenide; trifluoroacetic acid;
palladium on activated charcoal;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00140a025
- Guidance literature:
-
Multi-step reaction with 8 steps
1: PDC / dimethylformamide
3: H2 / Pd/C
4: KF(H2O)2
5: TFA / CH2Cl2
6: (benzotriazol-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate, diisopropylethylamine
7: TFA / CH2Cl2
8: (benzotriazol-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate, diisopropylethylamine
With
potassium fluoride; dipyridinium dichromate; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
palladium on activated charcoal;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00140a025