sodium cyanoborohydride

Base Information

Chemical Name:sodium cyanoborohydride
CAS No.:29012-60-0
Molecular Formula:CH₃BN*Na
Molecular Weight:62.8423
Hs Code.:

Synonyms:sodium cyanoborohydride

Suppliers and Price of sodium cyanoborohydride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of sodium cyanoborohydride

Chemical Property:

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Technology Process of sodium cyanoborohydride

There total 1 articles about sodium cyanoborohydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16940-66-2
sodium tetrahydroborate

: 74-90-8
hydrogen cyanide

: 773837-37-9
sodium cyanide

: 29012-60-0
sodium cyanoborohydride

: 29012-61-1
sodium cyanobis(trihydroborate)

: 25895-60-7
sodium cyanoborohydride

Guidance literature:: In tetrahydrofuran; byproducts: H2; react. in THF at 20°C; not isolated; detected by NMR and IR; Kinetics;
DOI:10.1016/S0277-5387(00)88147-4

Reference yield: 88.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 29012-60-0
sodium cyanoborohydride

: [N-(p-methoxyphenyl)amino]methylferrocene

: 881427-86-7
[(N-methyl-N-(4-methoxyphenyl))amino]methylferrocene

Guidance literature:: With glacial acetic acid; In water; acetonitrile; to stirred soln. of N-arylaminomethylferrocene and aq. soln. of formaldehyde in MeCN added NaCNBH3; 30 min later glacial acid added dropwise until pH value reached neutral; mixt. stirred at room temp. for 6 h; monitored by thin-layer chromy.; solvent removed (vac.); NaOH added; extd. (Et2O); org. layer dried (Na2SO4); recrystd.; purified by chromy. (silica gel, ethyl acetate-hexane); elem. anal.;
DOI:10.1016/j.jorganchem.2005.10.056

Reference yield: 87.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 29012-60-0
sodium cyanoborohydride

: N-(phenyl)aminomethylferrocene

: [(N-methyl-N-phenyl)amino]methylferrocene

Guidance literature:: With glacial acetic acid; In water; acetonitrile; to stirred soln. of N-arylaminomethylferrocene and aq. soln. of formaldehyde in MeCN added NaCNBH3; 30 min later glacial acid added dropwise until pH value reached neutral; mixt. stirred at room temp. for 6 h; monitored by thin-layer chromy.; solvent removed (vac.); NaOH added; extd. (Et2O); org. layer dried (Na2SO4); recrystd.; purified by chromy. (silica gel, ethyl acetate-hexane); elem. anal.;
DOI:10.1016/j.jorganchem.2005.10.056