phosphorous acid benzyl ester 2-cyano-ethyl ester 3,7,11,15-tetramethyl-hexadecyl ester

Base Information

Chemical Name:phosphorous acid benzyl ester 2-cyano-ethyl ester 3,7,11,15-tetramethyl-hexadecyl ester
CAS No.:314740-79-9
Molecular Formula:C₃₀H₅₂NO₃P
Molecular Weight:505.722
Hs Code.:

Synonyms:phosphorous acid benzyl ester 2-cyano-ethyl ester 3,7,11,15-tetramethyl-hexadecyl ester

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Chemical Property of phosphorous acid benzyl ester 2-cyano-ethyl ester 3,7,11,15-tetramethyl-hexadecyl ester

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Technology Process of phosphorous acid benzyl ester 2-cyano-ethyl ester 3,7,11,15-tetramethyl-hexadecyl ester

There total 4 articles about phosphorous acid benzyl ester 2-cyano-ethyl ester 3,7,11,15-tetramethyl-hexadecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7541-49-3,844467-91-0
3,7,11,15-tetramethyl-2-hexadecen-1-ol

: 314740-79-9
phosphorous acid benzyl ester 2-cyano-ethyl ester 3,7,11,15-tetramethyl-hexadecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / PtO₂*H₂O / tetrahydrofuran / 20 h / 760.05 Torr

2: tetrazole / acetonitrile / 1.5 h

With 1H-tetrazole; hydrogen; platinum(IV) oxide; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ja0123958

Reference yield:

: 645-72-7
3,7,11,15-tetramethyl-hexadecanol

: 196197-29-2
O-benzyl-O-β-cyanoethyl-N,N-diisopropylphosphoramidite

: 314740-79-9
phosphorous acid benzyl ester 2-cyano-ethyl ester 3,7,11,15-tetramethyl-hexadecyl ester

Guidance literature:: With 1H-tetrazole; In acetonitrile; for 1.5h;
DOI:10.1021/ol006725p DOI:10.1021/ja0123958

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 314740-79-9
phosphorous acid benzyl ester 2-cyano-ethyl ester 3,7,11,15-tetramethyl-hexadecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / Hunig's base / 1 h / 20 °C

2: tetrazole / acetonitrile / 1.5 h

With 1H-tetrazole; N-ethyl-N,N-diisopropylamine; In acetonitrile;
DOI:10.1021/ja0123958