benzyl 2-cyanoethyl 3,7,11,15-tetramethylhexadecylphosphate

Base Information

Chemical Name:benzyl 2-cyanoethyl 3,7,11,15-tetramethylhexadecylphosphate
CAS No.:314740-80-2
Molecular Formula:C₃₀H₅₂NO₄P
Molecular Weight:521.721
Hs Code.:

Synonyms:benzyl 2-cyanoethyl 3,7,11,15-tetramethylhexadecylphosphate

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Chemical Property of benzyl 2-cyanoethyl 3,7,11,15-tetramethylhexadecylphosphate

Chemical Property:

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Technology Process of benzyl 2-cyanoethyl 3,7,11,15-tetramethylhexadecylphosphate

There total 6 articles about benzyl 2-cyanoethyl 3,7,11,15-tetramethylhexadecylphosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7541-49-3,844467-91-0
3,7,11,15-tetramethyl-2-hexadecen-1-ol

: 314740-80-2
benzyl 2-cyanoethyl 3,7,11,15-tetramethylhexadecylphosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / H₂ / PtO₂*H₂O / tetrahydrofuran / 20 h / 760.05 Torr

2: tetrazole / acetonitrile / 1.5 h

3: 498 mg / tert-butyl hydroperoxide / acetonitrile; decane / 1 h

With 1H-tetrazole; tert.-butylhydroperoxide; hydrogen; platinum(IV) oxide; In tetrahydrofuran; decane; acetonitrile;
DOI:10.1021/ja0123958

Reference yield:

: 314740-79-9
phosphorous acid benzyl ester 2-cyano-ethyl ester 3,7,11,15-tetramethyl-hexadecyl ester

: 314740-80-2
benzyl 2-cyanoethyl 3,7,11,15-tetramethylhexadecylphosphate

Guidance literature:: With tert.-butylhydroperoxide; In decane; acetonitrile; for 1h;
DOI:10.1021/ol006725p DOI:10.1021/ja0123958

Reference yield:

: 645-72-7
3,7,11,15-tetramethyl-hexadecanol

: 314740-80-2
benzyl 2-cyanoethyl 3,7,11,15-tetramethylhexadecylphosphate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrazole / acetonitrile / 1.5 h

2: 498 mg / tert-butyl hydroperoxide / acetonitrile; decane / 1 h

With 1H-tetrazole; tert.-butylhydroperoxide; In decane; acetonitrile;
DOI:10.1021/ol006725p DOI:10.1021/ja0123958