3-amino-N,4-dimethylbenzamide

Base Information

Chemical Name:3-amino-N,4-dimethylbenzamide
CAS No.:54884-19-4
Molecular Formula:C₉H₁₂N₂O
Molecular Weight:164.207
Hs Code.:
European Community (EC) Number:696-417-6
DSSTox Substance ID:DTXSID90504229
Wikidata:Q82358567
Mol file:54884-19-4.mol

Synonyms:3-amino-N,4-dimethylbenzamide;54884-19-4;MFCD09045349;SCHEMBL2297552;3-Amino-4,N-dimethyl-benzamide;DTXSID90504229;NXFCCUBWWTWZGE-UHFFFAOYSA-N;AKOS000113224;BS-38125;SY168088;3-Amino-N,4-dimethylbenzamide, AldrichCPR;CS-0117132;FT-0739419;EN300-33450;F87986;Z239124756

Suppliers and Price of 3-amino-N,4-dimethylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-amino-N,4-dimethylbenzamide
100mg
$ 65.00

Sigma-Aldrich
3-Amino-N,4-dimethylbenzamide Aldrich
1g
$ 258.00

ChemBridge Corporation
3-amino-N,4-dimethylbenzamide 95%
200 μmol
$ 49.00

American Custom Chemicals Corporation
3-AMINO-N,4-DIMETHYLBENZAMIDE 95.00%
5G
$ 1548.26

American Custom Chemicals Corporation
3-AMINO-N,4-DIMETHYLBENZAMIDE 95.00%
2.5G
$ 1227.82

American Custom Chemicals Corporation
3-AMINO-N,4-DIMETHYLBENZAMIDE 95.00%
1G
$ 852.55

AK Scientific
3-Amino-N,4-dimethylbenzamide
250mg
$ 278.00

Total 7 raw suppliers

Chemical Property of 3-amino-N,4-dimethylbenzamide

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:325.0±35.0 °C(Predicted)
PKA:15.31±0.46(Predicted)
Density:1.106±0.06 g/cm3(Predicted)
XLogP3:0.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:164.094963011
Heavy Atom Count:12
Complexity:170

Purity/Quality:

98% ,99% , ^*data from raw suppliers

3-amino-N,4-dimethylbenzamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 36
Safety Statements: 26

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(C=C1)C(=O)NC)N

Technology Process of 3-amino-N,4-dimethylbenzamide

There total 4 articles about 3-amino-N,4-dimethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 2458-12-0
3-amino-p-toluic acid

: 2592-95-2
benzotriazol-1-ol

: 54884-19-4
3-amino-4-methylbenzoic acid methylamide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; methylamine; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); at 54 ℃; for 2h;

Reference yield:

: 329940-36-5
N-methyl-3-nitro-4-methylbenzamide

: 54884-19-4
3-amino-4-methylbenzoic acid methylamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 3h; under 2223.8 Torr;
DOI:10.1021/jm7009414

Reference yield:

: 10397-30-5
4-methyl-3-nitrobenzoyl chloride

: 54884-19-4
3-amino-4-methylbenzoic acid methylamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 20 °C

2: palladium 10% on activated carbon; hydrogen / ethanol / 20 °C

With palladium 10% on activated carbon; hydrogen; triethylamine; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2012.04.116