3-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]propan-1-ol

Base Information

Chemical Name:3-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]propan-1-ol
CAS No.:178610-72-5
Molecular Formula:C₁₉H₂₁NO₅
Molecular Weight:343.379
Hs Code.:

Synonyms:3-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]propan-1-ol

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Chemical Property of 3-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]propan-1-ol

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Technology Process of 3-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]propan-1-ol

There total 3 articles about 3-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 178610-71-4
ethyl 3-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]propionate

: 178610-72-5
3-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]propan-1-ol

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol; for 3h; Heating;
DOI:10.1021/jm010490l

Reference yield:

: 4-[2-(furan-2-yl)-5-methyl-4-oxazolylmethoxy]-3-methoxybenzaldehyde

: 178610-72-5
3-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]propan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / NaH / dimethylformamide / 1 h / 0 - 20 °C

2: 93 percent / H₂ / 5percent Pd/C / ethyl acetate / atmospheric pressure

3: 83 percent / NaBH₄ / methanol; tetrahydrofuran / 3 h / Heating

With sodium tetrahydroborate; hydrogen; sodium hydride; 5percent Pd/C; In tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide; 1: Horner-Emmons reaction;
DOI:10.1021/jm010490l

Reference yield:

: 178610-70-3
ethyl (E)-4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxycinnamate

: 178610-72-5
3-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]propan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / H₂ / 5percent Pd/C / ethyl acetate / atmospheric pressure

2: 83 percent / NaBH₄ / methanol; tetrahydrofuran / 3 h / Heating

With sodium tetrahydroborate; hydrogen; 5percent Pd/C; In tetrahydrofuran; methanol; ethyl acetate;
DOI:10.1021/jm010490l