C₂₅H₂₄Cl₂N₃O₆S⁽¹⁺⁾*I^(1-)

Base Information

Chemical Name:C₂₅H₂₄Cl₂N₃O₆S⁽¹⁺⁾*I^(1-)
CAS No.:1370638-15-5
Molecular Formula:C₂₅H₂₄Cl₂N₃O₆S*I
Molecular Weight:692.359
Hs Code.:

C<sub>25</sub>H<sub>24</sub>Cl<sub>2</sub>N<sub>3</sub>O<sub>6</sub>S<sup>(1+)</sup>*I<sup>(1-)</sup>

Synonyms:C₂₅H₂₄Cl₂N₃O₆S⁽¹⁺⁾*I^(1-)

Suppliers and Price of C₂₅H₂₄Cl₂N₃O₆S⁽¹⁺⁾*I^(1-)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₄Cl₂N₃O₆S⁽¹⁺⁾*I^(1-)

Chemical Property:

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Technology Process of C₂₅H₂₄Cl₂N₃O₆S⁽¹⁺⁾*I^(1-)

There total 12 articles about C₂₅H₂₄Cl₂N₃O₆S⁽¹⁺⁾*I^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 91177-27-4
7-(N-4-methylbenzamide)-3-(chloromethyl)-8-oxo-5-oxo-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid diphenylmethyl ester

: 1370638-15-5
C₂₅H₂₄Cl₂N₃O₆S⁽¹⁺⁾*I^(1-)

Guidance literature:: Multi-step reaction with 5 steps

1: tert-butylhypochlorite / methanol; dichloromethane / -45 °C

2: pyridine; phosphorus pentachloride / methanol; dichloromethane / -40 °C

3: pyridine; trichlorophosphate / methanol; dichloromethane / -40 - 0 °C

4: sodium iodide / dichloromethane; acetone / 0 °C

5: 3-methyl-phenol / 40 °C

With pyridine; tert-butylhypochlorite; phosphorus pentachloride; 3-methyl-phenol; sodium iodide; trichlorophosphate; In methanol; dichloromethane; acetone;
DOI:10.1016/j.cclet.2012.01.014

Reference yield:

: 17028-66-9
6β-(4-toluamido)penicillanic acid

: 1370638-15-5
C₂₅H₂₄Cl₂N₃O₆S⁽¹⁺⁾*I^(1-)

Guidance literature:: Multi-step reaction with 12 steps

1.1: pyridine; methanesulfonyl chloride / -5 - 10 °C

2.1: sodium tungstate; dihydrogen peroxide / 0 °C

3.1: chloro-trimethyl-silane; triethylamine / 10 °C

4.1: triphenylphosphine / ethyl acetate / 78 °C

5.1: chlorine; sodium hydrogencarbonate / water; ethyl acetate / 20 - 25 °C

5.2: 25 °C

6.1: pyridine; chlorine / dichloromethane

7.1: diethylamine / -20 °C

8.1: tert-butylhypochlorite / methanol; dichloromethane / -45 °C

9.1: pyridine; phosphorus pentachloride / methanol; dichloromethane / -40 °C

10.1: pyridine; trichlorophosphate / methanol; dichloromethane / -40 - 0 °C

11.1: sodium iodide / dichloromethane; acetone / 0 °C

12.1: 3-methyl-phenol / 40 °C

With pyridine; sodium tungstate; chloro-trimethyl-silane; tert-butylhypochlorite; phosphorus pentachloride; dihydrogen peroxide; chlorine; sodium hydrogencarbonate; methanesulfonyl chloride; 3-methyl-phenol; diethylamine; triethylamine; triphenylphosphine; sodium iodide; trichlorophosphate; In methanol; dichloromethane; water; ethyl acetate; acetone;
DOI:10.1016/j.cclet.2012.01.014

Reference yield:

: 82468-41-5
C₂₉H₂₈N₂O₅S

: 1370638-15-5
C₂₅H₂₄Cl₂N₃O₆S⁽¹⁺⁾*I^(1-)

Guidance literature:: Multi-step reaction with 9 steps

1.1: triphenylphosphine / ethyl acetate / 78 °C

2.1: chlorine; sodium hydrogencarbonate / water; ethyl acetate / 20 - 25 °C

2.2: 25 °C

3.1: pyridine; chlorine / dichloromethane

4.1: diethylamine / -20 °C

5.1: tert-butylhypochlorite / methanol; dichloromethane / -45 °C

6.1: pyridine; phosphorus pentachloride / methanol; dichloromethane / -40 °C

7.1: pyridine; trichlorophosphate / methanol; dichloromethane / -40 - 0 °C

8.1: sodium iodide / dichloromethane; acetone / 0 °C

9.1: 3-methyl-phenol / 40 °C

With pyridine; tert-butylhypochlorite; phosphorus pentachloride; chlorine; sodium hydrogencarbonate; 3-methyl-phenol; diethylamine; triphenylphosphine; sodium iodide; trichlorophosphate; In methanol; dichloromethane; water; ethyl acetate; acetone;
DOI:10.1016/j.cclet.2012.01.014