1-(4-tert-butylphenyl)-3,4,5-tris(4-(3-trimethylsilylphenyl)phenyl)benzene

Base Information

Chemical Name:1-(4-tert-butylphenyl)-3,4,5-tris(4-(3-trimethylsilylphenyl)phenyl)benzene
CAS No.:1609257-15-9
Molecular Formula:C₆₁H₆₆Si₃
Molecular Weight:883.452
Hs Code.:

Synonyms:1-(4-tert-butylphenyl)-3,4,5-tris(4-(3-trimethylsilylphenyl)phenyl)benzene

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Chemical Property of 1-(4-tert-butylphenyl)-3,4,5-tris(4-(3-trimethylsilylphenyl)phenyl)benzene

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Technology Process of 1-(4-tert-butylphenyl)-3,4,5-tris(4-(3-trimethylsilylphenyl)phenyl)benzene

There total 3 articles about 1-(4-tert-butylphenyl)-3,4,5-tris(4-(3-trimethylsilylphenyl)phenyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 957788-17-9
4-bromo-4-t-butyl-2',6'-bis(p-iodophenyl)-[1,1':4',1]terphenyl

: 177171-16-3
3-(trimethylsilyl)phenylboronic acid

: 1609257-11-5
1-(4-bromophenyl)-4-(4-tert-butylphenyl)-2,6-bis(4-(3-tri-methylsilylphenyl)phenyl)benzene

: 1609257-15-9
1-(4-tert-butylphenyl)-3,4,5-tris(4-(3-trimethylsilylphenyl)phenyl)benzene

: 1609257-13-7
C₅₂H₅₃ISi₂

Guidance literature:: With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; In tetrahydrofuran; at 50 ℃; for 96h; Glovebox; Schlenk technique;
DOI:10.1016/j.tet.2014.04.001

Reference yield: 12.0%

: 957788-17-9
4-bromo-4-t-butyl-2',6'-bis(p-iodophenyl)-[1,1':4',1]terphenyl

: 177171-16-3
3-(trimethylsilyl)phenylboronic acid

: 1609257-14-8
2-(4-bromophenyl)-5-(4-tert-butylphenyl)-1-(4-iodophenyl)-3-(4-(3-trimethylsilylphenyl)phenyl)benzene

: 1609257-11-5
1-(4-bromophenyl)-4-(4-tert-butylphenyl)-2,6-bis(4-(3-tri-methylsilylphenyl)phenyl)benzene

: 1609257-15-9
1-(4-tert-butylphenyl)-3,4,5-tris(4-(3-trimethylsilylphenyl)phenyl)benzene

: 1609257-13-7
C₅₂H₅₃ISi₂

Guidance literature:: With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; potassium hydroxide; In tetrahydrofuran; at 60 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1016/j.tet.2014.04.001

Reference yield: 2.0%

: 957788-17-9
4-bromo-4-t-butyl-2',6'-bis(p-iodophenyl)-[1,1':4',1]terphenyl

: 177171-16-3
3-(trimethylsilyl)phenylboronic acid

: 1609257-14-8
2-(4-bromophenyl)-5-(4-tert-butylphenyl)-1-(4-iodophenyl)-3-(4-(3-trimethylsilylphenyl)phenyl)benzene

: 1609257-11-5
1-(4-bromophenyl)-4-(4-tert-butylphenyl)-2,6-bis(4-(3-tri-methylsilylphenyl)phenyl)benzene

: 1609257-15-9
1-(4-tert-butylphenyl)-3,4,5-tris(4-(3-trimethylsilylphenyl)phenyl)benzene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In tetrahydrofuran; water; at 60 ℃; for 96h; Schlenk technique; Inert atmosphere;
DOI:10.1016/j.tet.2014.04.001