Technology Process of CH4O3S*C31H35Cl2N5O3
There total 10 articles about CH4O3S*C31H35Cl2N5O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
methanol;
at 20 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: thionyl chloride / 0.75 h / 60 °C
1.2: 0 - 20 °C
2.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C
3.1: triethylamine / N,N-dimethyl-formamide; acetonitrile / 2 h / 20 °C / Molecular sieve
4.1: methanol / 0.5 h / 20 °C
With
thionyl chloride; hydrogen; triethylamine;
palladium 10% on activated carbon;
In
methanol; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogen / 5 % platinum on carbon / tetrahydrofuran; methanol / 50 °C
2.1: thionyl chloride / 0.75 h / 60 °C
2.2: 0 - 20 °C
3.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C
4.1: triethylamine / N,N-dimethyl-formamide; acetonitrile / 2 h / 20 °C / Molecular sieve
5.1: methanol / 0.5 h / 20 °C
With
thionyl chloride; hydrogen; triethylamine;
5 % platinum on carbon; palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile;
