Thulium chloride--water (1/3/1)

Base Information

• Chemical Name: Thulium chloride--water (1/3/1)
• CAS No.: 19423-86-0
• Molecular Formula: Cl₃Tm*(x)H₂O
• Molecular Weight: 275.29
• Hs Code.: 2846902040
• DSSTox Substance ID: DTXSID00692924
• Mol file: 19423-86-0.mol

Synonyms:DTXSID00692924;Thulium chloride--water (1/3/1);AKOS022184712

Chemical Property of Thulium chloride--water (1/3/1)

Chemical Property:

• Melting Point: 824°C
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 0.00000
• Density: g/cm³
• LogP: -8.98800
• Sensitive.: Hygroscopic
• Water Solubility.: Soluble in water.
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 291.851342
• Heavy Atom Count: 5
• Complexity: 0

Purity/Quality:

97% ^*data from raw suppliers

Thulium(III) chloride hydrate (99.9%-Tm) (REO) ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Safety Statements: 26-36

MSDS Files:

Useful:

• Canonical SMILES: O.[Cl-].[Cl-].[Cl-].[Tm+3]
• Uses: ERBIUM CARBONATE HYDRATE is an important colourant in glasses and porcelain enamel glazes. High purity Erbium Carbonate is widely applied as dopant in making optical fibre and amplifier. It is particularly useful as an amplifier for fiber optic data transfer. Thulium(III) chloride hydrate is used in proteomics research. It is also used in the production of glass, phosphors and lasers. Further, it serves as an important dopant for fiber amplifiers. Further, it is also used to prepare thulium(III) oxide.

Technology Process of Thulium chloride--water (1/3/1)

There total 8 articles about Thulium chloride--water (1/3/1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

hydrogenchloride (7647-01-0,15364-23-5) + thulia + water (7732-18-5) → thulium(III) chloride hexahydrate (13778-39-7,19423-86-0)

Guidance literature:

In hydrogenchloride; Tm2O3 was heated with concd. aq. HCl; soln. was evapd. to dryness in vacuo at 50°C;

DOI:10.1016/j.ica.2003.11.011

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + thulia → thulium(III) chloride hexahydrate (13778-39-7,19423-86-0)

Guidance literature:

In hydrogenchloride; water; oxide dissoln. in H2O/HCl, excess water boiling off (stiring) until thick slurry obtained, slurry cooling to room temp., excess soln. filtrationoff; solid vac. treating (<1 torr) at 30-40°C (intermediate grinding and stirring);

Reference yield:

thulium(III) chloride hexahydrate (13778-39-7,19423-86-0) → TmCl3*H2O (114363-74-5,13778-39-7,19423-86-0)

Guidance literature:

With hydrogenchloride; In neat (no solvent); byproducts: H2O; sample dehydration in fluidized bed in Pyrex glass tube in Ar/HCl gas mixt. (12-14 l/min) at 80 or 135°C; gravimetric monitoring; Kinetics;

upstream raw materials:

hydrogenchloride

water

thulium(III) chloride hexahydrate

TmCl₃*3H₂O

Downstream raw materials:

(TmCl₂(((H₃C)2N)3PO)4)⁽¹⁺⁾*B(C₆H₅)4^(1-)=(TmCl₂(((H₃C)2N)3PO)4)(B(C₆H₅)4)

Tm(OOCC₆H₅)3

{Tm(C₆H₃(OH)(OCH₃)CHNC₁₀H₇)2Cl₂(H₂O)2}⁽¹⁺⁾*Cl^(1-)*H₂O={Tm(C₆H₃(OH)(OCH₃)CHNC₁₀H₇)2Cl₂(H₂O)2}Cl*H₂O

[Tm(III)Cl₂(triphenylphosphine oxide)4]PF₆

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