di-tert-butyl 4-amino>benzoyl-L-glutamate

Base Information

Chemical Name:di-tert-butyl 4-amino>benzoyl-L-glutamate
CAS No.:123724-55-0
Molecular Formula:C₂₆H₄₂N₂O₁₁S₂
Molecular Weight:622.758
Hs Code.:

di-tert-butyl 4-<bis<2-(mesyloxy)ethyl>amino>benzoyl-L-glutamate

Synonyms:di-tert-butyl 4-amino>benzoyl-L-glutamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-tert-butyl 4-amino>benzoyl-L-glutamate

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Technology Process of di-tert-butyl 4-amino>benzoyl-L-glutamate

There total 2 articles about di-tert-butyl 4-amino>benzoyl-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 123724-54-9
di-tert-butyl 4-benzoyl-L-glutamate

: 124-63-0
methanesulfonyl chloride

: 123724-56-1
di-tert-butyl 4-<(2-chloroethyl)<2-(mesyloxy)ethyl>amino>benzoyl-L-glutamate

: 123724-55-0
di-tert-butyl 4-amino>benzoyl-L-glutamate

Guidance literature:: With pyridine; 1.) 2 deg C, 20 min, 2.) 50 deg C, 10 min;
DOI:10.1021/jm00164a034

Reference yield:

: 76282-66-1
di-tert-butyl (S)-N-(p-aminobenzoyl)-glutamate

: 123724-55-0
di-tert-butyl 4-amino>benzoyl-L-glutamate

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / acetic acid / 48 h / Ambient temperature

2: 22 percent / acetic acid / 1.) 2 deg C, 20 min, 2.) 50 deg C, 10 min

With acetic acid;
DOI:10.1021/jm00164a034