2-<(1,4,4a,9,9a,10-Hexahydro-9,10-dioxo-1-anthryl)methyl>-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon

Base Information

Chemical Name:2-<(1,4,4a,9,9a,10-Hexahydro-9,10-dioxo-1-anthryl)methyl>-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon
CAS No.:104091-81-8
Molecular Formula:C₃₉H₃₉NO₁₄
Molecular Weight:745.737
Hs Code.:

Synonyms:2-<(1,4,4a,9,9a,10-Hexahydro-9,10-dioxo-1-anthryl)methyl>-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon

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Chemical Property of 2-<(1,4,4a,9,9a,10-Hexahydro-9,10-dioxo-1-anthryl)methyl>-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon

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Technology Process of 2-<(1,4,4a,9,9a,10-Hexahydro-9,10-dioxo-1-anthryl)methyl>-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon

There total 1 articles about 2-<(1,4,4a,9,9a,10-Hexahydro-9,10-dioxo-1-anthryl)methyl>-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 104153-51-7
(E)-2-(1,2,3,4,5-Pentaacetoxy-D-gluco-pentyl)-2-(2,4-pentadienyl)-4-phenyl-5(2H)-oxazolon

: 130-15-4
[1,4]naphthoquinone

: 104091-81-8
2-<(1,4,4a,9,9a,10-Hexahydro-9,10-dioxo-1-anthryl)methyl>-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 40h;

Reference yield:

: 104091-81-8
2-<(1,4,4a,9,9a,10-Hexahydro-9,10-dioxo-1-anthryl)methyl>-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon

: 104091-85-2
2-<(9,10-Dihydro-9,10-dioxo-1-anthryl)methyl>-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon

Guidance literature:: Multi-step reaction with 2 steps

1: NEt₃ / benzene / 3 h / Heating

2: DDQ / benzene / 3 h / Heating

With triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene;