1-benzyl-2,2-di(2-propenyl)pyrrolidine

Base Information

Chemical Name:1-benzyl-2,2-di(2-propenyl)pyrrolidine
CAS No.:457605-90-2
Molecular Formula:C₁₇H₂₃N
Molecular Weight:241.376
Hs Code.:

Synonyms:1-benzyl-2,2-di(2-propenyl)pyrrolidine

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Chemical Property of 1-benzyl-2,2-di(2-propenyl)pyrrolidine

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Technology Process of 1-benzyl-2,2-di(2-propenyl)pyrrolidine

There total 4 articles about 1-benzyl-2,2-di(2-propenyl)pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 40162-97-8
2,2-di(2-propenyl)pyrrolidine

: 100-39-0
benzyl bromide

: 457605-90-2
1-benzyl-2,2-di(2-propenyl)pyrrolidine

Guidance literature:: With potassium carbonate; In methanol; for 5h; Heating;
DOI:10.1023/A:1015864100939

Reference yield: 86.0%

: 5291-77-0
1-benzyl-2-pyrrolidone

: 1730-25-2
allylmagnesium bromide

: 457605-90-2
1-benzyl-2,2-di(2-propenyl)pyrrolidine

Guidance literature:: 1-benzyl-2-pyrrolidone; With trifluoromethylsulfonic anhydride; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -78 ℃; for 0.75h;

allylmagnesium bromide; In diethyl ether; dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/acs.joc.1c01572

Reference yield: 74.0%

: 5291-77-0
1-benzyl-2-pyrrolidone

: 925-90-6
ethylmagnesium bromide

: 1730-25-2
allylmagnesium bromide

: 1228468-98-1
2-allyl-1-benzyl-2-ethylpyrrolidine

: 457605-90-2
1-benzyl-2,2-di(2-propenyl)pyrrolidine

Guidance literature:: 1-benzyl-2-pyrrolidone; With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at -78 ℃; for 0.75h;

ethylmagnesium bromide; In diethyl ether; dichloromethane; at -78 - 20 ℃;

allylmagnesium bromide; In diethyl ether; dichloromethane; at 20 ℃; for 3h;
DOI:10.1002/anie.201000652