3-[3-(Dimethylamino)propyl]-4-[(1-methoxy-3-methyl-6-phenyl)-5-hexyl]sydnone

Base Information

Chemical Name:3-[3-(Dimethylamino)propyl]-4-[(1-methoxy-3-methyl-6-phenyl)-5-hexyl]sydnone
CAS No.:389574-42-9
Molecular Formula:C₂₁H₃₁N₃O₃
Molecular Weight:373.495
Hs Code.:

Synonyms:3-[3-(Dimethylamino)propyl]-4-[(1-methoxy-3-methyl-6-phenyl)-5-hexyl]sydnone

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Chemical Property of 3-[3-(Dimethylamino)propyl]-4-[(1-methoxy-3-methyl-6-phenyl)-5-hexyl]sydnone

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Technology Process of 3-[3-(Dimethylamino)propyl]-4-[(1-methoxy-3-methyl-6-phenyl)-5-hexyl]sydnone

There total 1 articles about 3-[3-(Dimethylamino)propyl]-4-[(1-methoxy-3-methyl-6-phenyl)-5-hexyl]sydnone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 389574-41-8
3-[3-(Dimethylamino)propyl]-4-[(1-hydroxy-3-methyl-6-phenyl)-5-hexyl]sydnone

: 74-88-4
methyl iodide

: 389574-42-9
3-[3-(Dimethylamino)propyl]-4-[(1-methoxy-3-methyl-6-phenyl)-5-hexyl]sydnone

Guidance literature:: 3-[3-(Dimethylamino)propyl]-4-[(1-hydroxy-3-methyl-6-phenyl)-5-hexyl]sydnone; With sodium hydride; In tetrahydrofuran; for 0.5h;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1055/s-2001-17517

Reference yield: 46.0%

: 389574-42-9
3-[3-(Dimethylamino)propyl]-4-[(1-methoxy-3-methyl-6-phenyl)-5-hexyl]sydnone

: 1-[3-(Dimethylamino)propyl]-7-methoxy-5-methyl-3-phenyl-1H-4,5,6,7-tetrahydroindazole

Guidance literature:: In xylene; at 130 ℃; for 22h;
DOI:10.1055/s-2001-17517

Reference yield:

: 389574-42-9
3-[3-(Dimethylamino)propyl]-4-[(1-methoxy-3-methyl-6-phenyl)-5-hexyl]sydnone

: 57614-23-0
1-[3-(Dimethylamino)propyl]-5-methyl-3-phenyl-1H-indazole

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / xylene / 22 h / 130 °C

2: 26 percent / HClO₄ / Pt/C / acetic acid / 40 h / Heating

With perchloric acid; platinum on activated charcoal; In acetic acid; xylene;
DOI:10.1055/s-2001-17517