2-[9-chloro-6-(3-hydroxy-3-methylbut-1-yn-1-yl)-1H-phenanthro[9,10-d]imidazol-2-yl]isophthalonitrile

Base Information

Chemical Name:2-[9-chloro-6-(3-hydroxy-3-methylbut-1-yn-1-yl)-1H-phenanthro[9,10-d]imidazol-2-yl]isophthalonitrile
CAS No.:892549-54-1
Molecular Formula:C₂₃H₁₀BrClN₄
Molecular Weight:457.716
Hs Code.:

Synonyms:2-[9-chloro-6-(3-hydroxy-3-methylbut-1-yn-1-yl)-1H-phenanthro[9,10-d]imidazol-2-yl]isophthalonitrile

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Chemical Property of 2-[9-chloro-6-(3-hydroxy-3-methylbut-1-yn-1-yl)-1H-phenanthro[9,10-d]imidazol-2-yl]isophthalonitrile

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Technology Process of 2-[9-chloro-6-(3-hydroxy-3-methylbut-1-yn-1-yl)-1H-phenanthro[9,10-d]imidazol-2-yl]isophthalonitrile

There total 18 articles about 2-[9-chloro-6-(3-hydroxy-3-methylbut-1-yn-1-yl)-1H-phenanthro[9,10-d]imidazol-2-yl]isophthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: C₂₁H₁₀BrClF₂N₂

: 143-33-9,25596-52-5
sodium cyanide

: 892549-54-1
2-[9-chloro-6-(3-hydroxy-3-methylbut-1-yn-1-yl)-1H-phenanthro[9,10-d]imidazol-2-yl]isophthalonitrile

Guidance literature:: C₂₁H₁₀BrClF₂N₂; sodium cyanide; copper(l) iodide; In N,N-dimethyl-formamide; at 120 ℃; for 45h;

With ammonia; water; In N,N-dimethyl-formamide; Product distribution / selectivity;

Reference yield: 97.0%

: 892550-46-8
9-bromo-6-chloro-2-(2,6-dibromophenyl)-1H-phenanthro[9,10-d]imidazole

: 143-33-9,25596-52-5
sodium cyanide

: 892549-54-1
2-[9-chloro-6-(3-hydroxy-3-methylbut-1-yn-1-yl)-1H-phenanthro[9,10-d]imidazol-2-yl]isophthalonitrile

Guidance literature:: With copper(l) iodide; In N,N-dimethyl-formamide; at 120 ℃; for 45h;

Reference yield: 89.5%

: C₂H₄O₂*C₂₁H₁₀BrClF₂N₂

: potassium ferrocyanide

: 892549-54-1
2-[9-chloro-6-(3-hydroxy-3-methylbut-1-yn-1-yl)-1H-phenanthro[9,10-d]imidazol-2-yl]isophthalonitrile

Guidance literature:: With 1,2-diamino-benzene; copper(l) iodide; In N,N-dimethyl-formamide; at 135 ℃; for 36h; Product distribution / selectivity;