<1(1R,3R,4R),1E,3(2S),3S>-3-<(piperidin-2-ylcarbonyl)oxy>-5-<(trimethylsilyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene

Base Information

Chemical Name:<1(1R,3R,4R),1E,3(2S),3S>-3-<(piperidin-2-ylcarbonyl)oxy>-5-<(trimethylsilyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene
CAS No.:136358-32-2
Molecular Formula:C₃₃H₆₅NO₅Si₂
Molecular Weight:612.054
Hs Code.:

<1(1R,3R,4R),1E,3(2S),3S>-3-<(piperidin-2-ylcarbonyl)oxy>-5-<(trimethylsilyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene

Synonyms:<1(1R,3R,4R),1E,3(2S),3S>-3-<(piperidin-2-ylcarbonyl)oxy>-5-<(trimethylsilyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene

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Chemical Property of <1(1R,3R,4R),1E,3(2S),3S>-3-<(piperidin-2-ylcarbonyl)oxy>-5-<(trimethylsilyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene

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Technology Process of <1(1R,3R,4R),1E,3(2S),3S>-3-<(piperidin-2-ylcarbonyl)oxy>-5-<(trimethylsilyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene

There total 5 articles about <1(1R,3R,4R),1E,3(2S),3S>-3-<(piperidin-2-ylcarbonyl)oxy>-5-<(trimethylsilyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.8%

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 136358-58-2
<1(1R,3R,4R),1E,3(2S),3S>-3-<<<-N-(tert-butoxycarbonyl)piperidin-2-yl>carbonyl>oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-penten-5-ol

: 136358-32-2
<1(1R,3R,4R),1E,3(2S),3S>-3-<(piperidin-2-ylcarbonyl)oxy>-5-<(trimethylsilyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield:

: 92156-87-1
2,2-dimethyl-3-(4-methoxyphenylmethoxy)propionaldehyde

: 136358-32-2
<1(1R,3R,4R),1E,3(2S),3S>-3-<(piperidin-2-ylcarbonyl)oxy>-5-<(trimethylsilyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene

Guidance literature:: Multi-step reaction with 4 steps

2: 91.6 percent / 4-pyrrolidinopyridine, diisopropylcarbodiimide / CH₂Cl₂ / 1 h / -20 °C

3: 80.5 percent / DDQ, H₂O / CH₂Cl₂

4: 80.8 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 0 °C

With 2,6-dimethylpyridine; water; 4-pyrrolidin-1-ylpyridine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; diisopropyl-carbodiimide; In dichloromethane;

Reference yield:

: 122948-78-1
(1R,2R,4R)-4-<(E)-2-bromo-1-propen-1-yl>-2-methoxy-1-<(triisopropylsilyl)oxy>cyclohexane

: 136358-32-2
<1(1R,3R,4R),1E,3(2S),3S>-3-<(piperidin-2-ylcarbonyl)oxy>-5-<(trimethylsilyl)oxy>-1-<3-methoxy-4-<(triisopropylsilyl)oxy>cyclohex-1-yl>-2,4,4-trimethyl-1-pentene

Guidance literature:: Multi-step reaction with 4 steps

2: 91.6 percent / 4-pyrrolidinopyridine, diisopropylcarbodiimide / CH₂Cl₂ / 1 h / -20 °C

3: 80.5 percent / DDQ, H₂O / CH₂Cl₂

4: 80.8 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 0 °C

With 2,6-dimethylpyridine; water; 4-pyrrolidin-1-ylpyridine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; diisopropyl-carbodiimide; In dichloromethane;