benzyl 2-iodo-4-methylphenyl ether

Base Information

• Chemical Name: benzyl 2-iodo-4-methylphenyl ether
• CAS No.: 100717-11-1
• Molecular Formula: C₁₄H₁₃IO
• Molecular Weight: 324.161

Synonyms:benzyl 2-iodo-4-methylphenyl ether

Chemical Property of benzyl 2-iodo-4-methylphenyl ether

Chemical Property:

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Technology Process of benzyl 2-iodo-4-methylphenyl ether

There total 2 articles about benzyl 2-iodo-4-methylphenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2-iodo-4-methylphenol (16188-57-1) + benzyl bromide (100-39-0) → benzyl 2-iodo-4-methylphenyl ether (100717-11-1)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 40 - 50 ℃; for 12h;

DOI:10.1080/10426500802253090

Reference yield: 54.0%

4-methylphenyl benzyl ether (834-25-3) → benzyl 2-iodo-4-methylphenyl ether (100717-11-1)

Guidance literature:

With iodine; silver trifluoroacetate; In dichloromethane;

Reference yield: 74.0%

2,2-difluoro-2-(fluorosulfonyl)acetate (680-15-9) + benzyl 2-iodo-4-methylphenyl ether (100717-11-1) → benzyl 4-methyl-2-trifluoromethylphenyl ether (1204817-23-1)

Guidance literature:

With copper(l) iodide; In N,N-dimethyl-formamide; at 80 ℃; for 24h;

DOI:10.1080/10426500802253090

upstream raw materials:

4-methylphenyl benzyl ether

2-iodo-4-methylphenol

benzyl bromide

Downstream raw materials:

benzyl 4-methyl-2-trifluoromethylphenyl ether

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