meso-N,N'-bis(4-methoxybenzyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine

Base Information

• Chemical Name: meso-N,N'-bis(4-methoxybenzyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine
• CAS No.: 730992-58-2
• Molecular Formula: C₃₀H₂₂F₁₀N₂O₂
• Molecular Weight: 632.501
• Mol file: 730992-58-2.mol

Synonyms:meso-N,N'-bis(4-methoxybenzyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine

Chemical Property of meso-N,N'-bis(4-methoxybenzyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of meso-N,N'-bis(4-methoxybenzyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine

There total 3 articles about meso-N,N'-bis(4-methoxybenzyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

(E)-4-methoxy-N-(pentafluorobenzylidene)benzylamine (730992-49-1) → meso-N,N'-bis(4-methoxybenzyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine (730992-58-2) + (+/-)-N,N'-bis(4-methoxybenzyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine

Guidance literature:

With copper; toluene-4-sulfonic acid; zinc; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1246/bcsj.77.1001

Reference yield:

perfluorobenzaldehyde (653-37-2) → meso-N,N'-bis(4-methoxybenzyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine (730992-58-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / CH₂Cl₂ / 3 h / 20 °C

2: 13 percent / Zn-Cu; p-TsOH*H₂O / tetrahydrofuran / 2 h / 20 °C

With copper; toluene-4-sulfonic acid; zinc; In tetrahydrofuran; dichloromethane;

DOI:10.1246/bcsj.77.1001

Reference yield:

4-methoxy-benzylamine (2393-23-9) → meso-N,N'-bis(4-methoxybenzyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine (730992-58-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / CH₂Cl₂ / 3 h / 20 °C

2: 13 percent / Zn-Cu; p-TsOH*H₂O / tetrahydrofuran / 2 h / 20 °C

With copper; toluene-4-sulfonic acid; zinc; In tetrahydrofuran; dichloromethane;

DOI:10.1246/bcsj.77.1001

upstream raw materials:

(E)-4-methoxy-N-(pentafluorobenzylidene)benzylamine

perfluorobenzaldehyde

4-methoxy-benzylamine