O-(methyl 3-O-benzyl-2,4-di-O-pivaloyl-α,β-L-idopyranosyluronate) trichloroacetimidate

Base Information

Chemical Name:O-(methyl 3-O-benzyl-2,4-di-O-pivaloyl-α,β-L-idopyranosyluronate) trichloroacetimidate
CAS No.:882167-09-1
Molecular Formula:C₂₆H₃₄Cl₃NO₉
Molecular Weight:610.916
Hs Code.:

Synonyms:O-(methyl 3-O-benzyl-2,4-di-O-pivaloyl-α,β-L-idopyranosyluronate) trichloroacetimidate

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Chemical Property of O-(methyl 3-O-benzyl-2,4-di-O-pivaloyl-α,β-L-idopyranosyluronate) trichloroacetimidate

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Technology Process of O-(methyl 3-O-benzyl-2,4-di-O-pivaloyl-α,β-L-idopyranosyluronate) trichloroacetimidate

There total 3 articles about O-(methyl 3-O-benzyl-2,4-di-O-pivaloyl-α,β-L-idopyranosyluronate) trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 882167-07-9
methyl (dimethylthexylsilyl 3-O-benzyl-2,4-di-O-pivaloyl-β-L-idopyranoside)uronate

: 882167-09-1
O-(methyl 3-O-benzyl-2,4-di-O-pivaloyl-α,β-L-idopyranosyluronate) trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / HF*Py / tetrahydrofuran / 48 h / -10 - 0 °C

2: 90 percent / K₂CO₃ / CH₂Cl₂ / 16 h / 20 °C

With potassium carbonate; pyridine hydrogenfluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja057584v

Reference yield:

: 3282-30-2
pivaloyl chloride

: 882167-09-1
O-(methyl 3-O-benzyl-2,4-di-O-pivaloyl-α,β-L-idopyranosyluronate) trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / pyridine; DMAP / 12 h / 20 °C

2: 80 percent / HF*Py / tetrahydrofuran / 48 h / -10 - 0 °C

3: 90 percent / K₂CO₃ / CH₂Cl₂ / 16 h / 20 °C

With pyridine; dmap; potassium carbonate; pyridine hydrogenfluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja057584v

Reference yield:

: 243982-79-8
methyl (dimethylthexylsilyl 3-O-benzyl-β-L-idopyranoside)uronate

: 882167-09-1
O-(methyl 3-O-benzyl-2,4-di-O-pivaloyl-α,β-L-idopyranosyluronate) trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / pyridine; DMAP / 12 h / 20 °C

2: 80 percent / HF*Py / tetrahydrofuran / 48 h / -10 - 0 °C

3: 90 percent / K₂CO₃ / CH₂Cl₂ / 16 h / 20 °C

With pyridine; dmap; potassium carbonate; pyridine hydrogenfluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja057584v