Hydrazinecarboxylic acid, 1-methyl-1-phenylethyl ester (9CI)

Base Information

Chemical Name:Hydrazinecarboxylic acid, 1-methyl-1-phenylethyl ester (9CI)
CAS No.:18597-93-8
Molecular Formula:C10H14 N2 O2
Molecular Weight:194.233
Hs Code.:2928000090
Mol file:18597-93-8.mol

Synonyms:Carbazicacid, a,a-dimethylbenzyl ester (8CI); Benzyl alcohol, a,a-dimethyl-, carbazate; 1-Methyl-1-phenethyl carbazate;a,a-Dimethylbenzyl carbazate

Suppliers and Price of Hydrazinecarboxylic acid, 1-methyl-1-phenylethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Hydrazinecarboxylic acid, 1-methyl-1-phenylethyl ester (9CI)

Chemical Property:

PSA：67.84000
LogP:2.42630

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Hydrazinecarboxylic acid, 1-methyl-1-phenylethyl ester (9CI)

There total 4 articles about Hydrazinecarboxylic acid, 1-methyl-1-phenylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 53933-09-8
2-phenylisopropyloxycarbonyl phenyl carbonate

: 18597-93-8
cumyl carbazate

Guidance literature:: With hydrazine hydrate; In water; for 18h;
DOI:10.1021/acs.jmedchem.6b00108

Reference yield: 82.0%

: 617-94-7
1-methyl-1-phenylethyl alcohol

: 1885-14-9
phenyl chloroformate

: 18597-93-8
cumyl carbazate

Guidance literature:: 1-methyl-1-phenylethyl alcohol; phenyl chloroformate; With pyridine; In dichloromethane; at 0 - 20 ℃; for 18h;

With hydrazine hydrate; at 20 ℃; for 18h;

Reference yield:

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 18597-93-8
cumyl carbazate

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 2 h / 0 - 45 °C

2: pyridine / dichloromethane / -5 - 0 °C

3: hydrazine hydrate / water / 18 h

With pyridine; hydrazine hydrate; In diethyl ether; dichloromethane; water;
DOI:10.1021/acs.jmedchem.6b00108