3-phenoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

Base Information

Chemical Name:3-phenoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether
CAS No.:1487429-03-7
Molecular Formula:C₁₉H₂₂O₄
Molecular Weight:314.381
Hs Code.:

Synonyms:3-phenoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

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Chemical Property of 3-phenoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

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Technology Process of 3-phenoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

There total 3 articles about 3-phenoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1487429-02-6
2-(3-iodophenoxy)ethyl tetrahydro-2H-pyran-2-yl ether

: 108-95-2,27073-41-2
phenol

: 1487429-03-7
3-phenoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

Guidance literature:: 2-(3-iodophenoxy)ethyl tetrahydro-2H-pyran-2-yl ether; phenol; With 2-Picolinic acid; potassium phosphate; copper(l) iodide; Inert atmosphere;

With dimethyl sulfoxide; at 80 ℃; for 24h;
DOI:10.1016/j.ejmech.2013.09.009

Reference yield:

: 626-02-8
3-Iodophenol

: 1487429-03-7
3-phenoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 0.5 h / 20 °C

1.2: 16 h / 20 °C

2.1: copper(l) iodide; 2-Picolinic acid; potassium phosphate / Inert atmosphere

2.2: 24 h / 80 °C

With 2-Picolinic acid; potassium phosphate; copper(l) iodide; potassium hydroxide; In dimethyl sulfoxide;
DOI:10.1016/j.ejmech.2013.09.009

Reference yield:

: 17739-45-6,59146-56-4
2-(2-bromoethoxy)tetrahydropyran

: 1487429-03-7
3-phenoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 0.5 h / 20 °C

1.2: 16 h / 20 °C

2.1: copper(l) iodide; 2-Picolinic acid; potassium phosphate / Inert atmosphere

2.2: 24 h / 80 °C

With 2-Picolinic acid; potassium phosphate; copper(l) iodide; potassium hydroxide; In dimethyl sulfoxide;
DOI:10.1016/j.ejmech.2013.09.009