Technology Process of C38H34O7
There total 1 articles about C38H34O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1-(2-(benzyloxy)-6-hydroxy-4-(methoxymethoxy)phenyl)ethan-1-one;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 0 - 20 ℃;
for 0.5h;
3,4-dibenzyloxybenzaldehyde;
In
N,N-dimethyl-formamide; mineral oil;
at 0 - 20 ℃;
for 1.08333h;
With
water;
In
N,N-dimethyl-formamide; mineral oil;
at 0 ℃;
DOI:10.1016/j.tetlet.2012.01.054
- Guidance literature:
-
With
sodium tetrahydroborate; cerium(III) chloride heptahydrate;
In
tetrahydrofuran; ethanol;
at -40 - 0 ℃;
for 5.08333h;
DOI:10.1016/j.tetlet.2012.01.054
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / tetrahydrofuran; ethanol / 5.08 h / -40 - 0 °C
2: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C
3: AD-mix-α; methanesulfonamide; water / tetrahydrofuran; tert-butyl alcohol / 16 h / 0 - 20 °C
4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1 h / 0 °C
5: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane / 2 h / 65 °C
With
1H-imidazole; sodium tetrahydroborate; methanesulfonamide; cerium(III) chloride heptahydrate; AD-mix-α; tetrabutyl ammonium fluoride; water; pyridinium p-toluenesulfonate; acetic acid;
In
tetrahydrofuran; ethanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; tert-butyl alcohol;
3: Sharpless dihydroxylation;
DOI:10.1016/j.tetlet.2012.01.054
