methyl 2-O-benzoyl-3,5-di-O-benzyl-2-C-β-methoxymethyl-α-D-ribofuranoside

Base Information

Chemical Name:methyl 2-O-benzoyl-3,5-di-O-benzyl-2-C-β-methoxymethyl-α-D-ribofuranoside
CAS No.:948838-08-2
Molecular Formula:C₂₉H₃₂O₇
Molecular Weight:492.569
Hs Code.:

Synonyms:methyl 2-O-benzoyl-3,5-di-O-benzyl-2-C-β-methoxymethyl-α-D-ribofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-O-benzoyl-3,5-di-O-benzyl-2-C-β-methoxymethyl-α-D-ribofuranoside

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Technology Process of methyl 2-O-benzoyl-3,5-di-O-benzyl-2-C-β-methoxymethyl-α-D-ribofuranoside

There total 6 articles about methyl 2-O-benzoyl-3,5-di-O-benzyl-2-C-β-methoxymethyl-α-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 948838-03-7
methyl 3,5-di-O-benzyl-2-C-β-methoxymethyl-α-D-ribofuranoside

: 98-88-4
benzoyl chloride

: 948838-08-2
methyl 2-O-benzoyl-3,5-di-O-benzyl-2-C-β-methoxymethyl-α-D-ribofuranoside

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 72h;
DOI:10.1021/ol071075b

Reference yield:

: 80795-53-5
(2S,3R,4S,5R)-4-(benzyloxy)-5-((benzyloxy)methyl)-2-methoxytetrahydrofuran-3-ol

: 948838-08-2
methyl 2-O-benzoyl-3,5-di-O-benzyl-2-C-β-methoxymethyl-α-D-ribofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 97 percent / Dess-Martin periodinane / CH₂Cl₂ / 24 h / 20 °C

2.1: HgCl₂; magnesium / tetrahydrofuran / 2 h / -30 - -23 °C

2.2: 50 percent / tetrahydrofuran / 49 h / -78 - 20 °C

3.1: 64 percent / DMAP; triethylamine / CH₂Cl₂ / 72 h / 20 °C

With dmap; Dess-Martin periodane; magnesium; triethylamine; mercury dichloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol071075b

Reference yield:

: 885592-69-8
(2S,4R,5R)-4-(benzyloxy)-5-((benzyloxy)methyl)-2-methoxydihydrofuran-3(2H)-one

: 948838-08-2
methyl 2-O-benzoyl-3,5-di-O-benzyl-2-C-β-methoxymethyl-α-D-ribofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: HgCl₂; magnesium / tetrahydrofuran / 2 h / -30 - -23 °C

1.2: 50 percent / tetrahydrofuran / 49 h / -78 - 20 °C

2.1: 64 percent / DMAP; triethylamine / CH₂Cl₂ / 72 h / 20 °C

With dmap; magnesium; triethylamine; mercury dichloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol071075b