(S)-3-<(phenylmethoxy)carbonyl>-4-oxazolidinecarboxylic acid methyl ester

Base Information

Chemical Name:(S)-3-<(phenylmethoxy)carbonyl>-4-oxazolidinecarboxylic acid methyl ester
CAS No.:126111-22-6
Molecular Formula:C₁₃H₁₅NO₅
Molecular Weight:265.266
Hs Code.:

Synonyms:(S)-3-<(phenylmethoxy)carbonyl>-4-oxazolidinecarboxylic acid methyl ester

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Chemical Property of (S)-3-<(phenylmethoxy)carbonyl>-4-oxazolidinecarboxylic acid methyl ester

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Technology Process of (S)-3-<(phenylmethoxy)carbonyl>-4-oxazolidinecarboxylic acid methyl ester

There total 2 articles about (S)-3-<(phenylmethoxy)carbonyl>-4-oxazolidinecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 67-56-1
methanol

: 97534-82-2,97534-84-4
(4S)-3-[(benzyloxy)carbonyl]-1,3-oxazolidine-4-carboxylic acid

: 126111-22-6
(S)-3-<(phenylmethoxy)carbonyl>-4-oxazolidinecarboxylic acid methyl ester

Guidance literature:: methanol; (4S)-3-[(benzyloxy)carbonyl]-1,3-oxazolidine-4-carboxylic acid; With thionyl chloride; at 0 - 20 ℃;

With sodium hydrogencarbonate; In methanol; water;

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 97534-82-2,97534-84-4
(4S)-3-[(benzyloxy)carbonyl]-1,3-oxazolidine-4-carboxylic acid

: 126111-22-6
(S)-3-<(phenylmethoxy)carbonyl>-4-oxazolidinecarboxylic acid methyl ester

Guidance literature:: In diethyl ether; at 0 ℃; Yield given;
DOI:10.1021/jm00167a028

Reference yield: 91.0%

: 64154-78-5
4-benzyloxy-5-methoxy-2-nitrobenzoyl chloride

: 126111-22-6
(S)-3-<(phenylmethoxy)carbonyl>-4-oxazolidinecarboxylic acid methyl ester

: 1239587-39-3
C₂₀H₂₀N₂O₈

Guidance literature:: (S)-3-<(phenylmethoxy)carbonyl>-4-oxazolidinecarboxylic acid methyl ester; With hydrogen; triethylamine; Pearlman's catalist; In ethyl acetate; at 20 ℃; for 2h;

4-benzyloxy-5-methoxy-2-nitrobenzoyl chloride; With triethylamine; In tetrahydrofuran; ethyl acetate; at 0 ℃; for 3h;