(3R,5S)-3,5-dihydroxy-N,N-dimethyl-6-(1-phenyl-1H-tetrazol-5-ylthio)hexanamide

Base Information

Chemical Name:(3R,5S)-3,5-dihydroxy-N,N-dimethyl-6-(1-phenyl-1H-tetrazol-5-ylthio)hexanamide
CAS No.:1332363-94-6
Molecular Formula:C₁₅H₂₁N₅O₃S
Molecular Weight:351.429
Hs Code.:

Synonyms:(3R,5S)-3,5-dihydroxy-N,N-dimethyl-6-(1-phenyl-1H-tetrazol-5-ylthio)hexanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,5S)-3,5-dihydroxy-N,N-dimethyl-6-(1-phenyl-1H-tetrazol-5-ylthio)hexanamide

Chemical Property:

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Technology Process of (3R,5S)-3,5-dihydroxy-N,N-dimethyl-6-(1-phenyl-1H-tetrazol-5-ylthio)hexanamide

There total 3 articles about (3R,5S)-3,5-dihydroxy-N,N-dimethyl-6-(1-phenyl-1H-tetrazol-5-ylthio)hexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1332363-93-5
(S)-5-hydroxy-N,N-dimethyl-3-oxo-6-(1-phenyl-1H-tetrazol-5-ylthio)hexanamide

: 1332363-94-6
(3R,5S)-3,5-dihydroxy-N,N-dimethyl-6-(1-phenyl-1H-tetrazol-5-ylthio)hexanamide

Guidance literature:: With methanol; sodium tetrahydroborate; diethoxymethylborane; at -60 ℃;

Reference yield:

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 1332363-94-6
(3R,5S)-3,5-dihydroxy-N,N-dimethyl-6-(1-phenyl-1H-tetrazol-5-ylthio)hexanamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / toluene / 80 - 85 °C

2.1: diisopropylamine; N-butylamine / tetrahydrofuran / 0.5 h / -10 °C

2.2: 2 h / -40 °C

3.1: sodium tetrahydroborate; methanol; diethoxymethylborane / -60 °C

With methanol; sodium tetrahydroborate; diethoxymethylborane; N-butylamine; triethylamine; diisopropylamine; In tetrahydrofuran; toluene;

Reference yield:

: 1332363-92-4
(S)-ethyl-3-hydroxy-4-(1-phenyl-1H-tetrazol-5-ylthio)butanoate

: 1332363-94-6
(3R,5S)-3,5-dihydroxy-N,N-dimethyl-6-(1-phenyl-1H-tetrazol-5-ylthio)hexanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisopropylamine; N-butylamine / tetrahydrofuran / 0.5 h / -10 °C

1.2: 2 h / -40 °C

2.1: sodium tetrahydroborate; methanol; diethoxymethylborane / -60 °C

With methanol; sodium tetrahydroborate; diethoxymethylborane; N-butylamine; diisopropylamine; In tetrahydrofuran;