Benzenesulfonamide, N,N'-1,6-hexanediylbis[4-methyl-

Base Information

• Chemical Name: Benzenesulfonamide, N,N'-1,6-hexanediylbis[4-methyl-
• CAS No.: 69762-22-7
• Molecular Formula: C20H28 N2 O4 S2
• Molecular Weight: 424.585
• NSC Number: 137866
• DSSTox Substance ID: DTXSID20300615
• Nikkaji Number: J2.768.856J
• Wikidata: Q82043824
• ChEMBL ID: CHEMBL1875589

Synonyms:Benzenesulfonamide, N,N'-1,6-hexanediylbis[4-methyl-;MLS002920438;69762-22-7;NSC137866;SCHEMBL7095731;CHEMBL1875589;DTXSID20300615;STK037962;AKOS000493883;NSC-137866;SMR001798030;Benzenesulfonamide,N'-1,6-hexanediylbis[4-methyl-;N,N'-hexane-1,6-diylbis(4-methylbenzenesulfonamide)

Chemical Property of Benzenesulfonamide, N,N'-1,6-hexanediylbis[4-methyl-

Chemical Property:

• Boiling Point: 591.5°Cat760mmHg
• Flash Point: 311.5°C
• Density: 1.212g/cm³
• XLogP3: 3.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 11
• Exact Mass: 424.14904973
• Heavy Atom Count: 28
• Complexity: 579

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)S(=O)(=O)NCCCCCCNS(=O)(=O)C2=CC=C(C=C2)C

Technology Process of Benzenesulfonamide, N,N'-1,6-hexanediylbis[4-methyl-

There total 3 articles about Benzenesulfonamide, N,N'-1,6-hexanediylbis[4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1,6-Hexanediamine (124-09-4) + p-toluenesulfonyl chloride (98-59-9) → N,N'-ditosyl-1,6-diaminohexane (69762-22-7)

Guidance literature:

With N,N'-dimethylaminopyridine; triethylamine; In dichloromethane; for 3h; Ambient temperature;

Reference yield:

1 ,6-dibromohexane (629-03-8) + toluene-4-sulfonamide (70-55-3) → N,N'-ditosyl-1,6-diaminohexane (69762-22-7)

Guidance literature:

With potassium hydroxide;

Reference yield:

→ N,N'-ditosyl-1,6-diaminohexane (69762-22-7)

Guidance literature:

p-Toluolsulfochlorid , Hexamethylendiamin <2h, 40-60grad>;

upstream raw materials:

1,6-Hexanediamine

p-toluenesulfonyl chloride

1 ,6-dibromohexane

toluene-4-sulfonamide

Downstream raw materials:

N,N'-bis<6-(2-tetrahydropyranyloxy)hexyl>-N,N'-di-p-toluenesulfonyl-1,6-hexanediamine

1,8,15,22-tetra-p-toluenesulfonyltetraazacyclooctacontane

N²,N⁹-di-p-toluenesulfonyl-15-hydroxy-16-hydroxymethyl-15,16'-O-isopropylidene-2,9-diaza<10>(2,5)pyridinophane

N²,N⁹-Di-p-tosyl-15-hydroxy-16-hydroxymethyl-15,16'-O-isopropylidene-12-methyl-2,9-diaza<10>(2,5)pyridinophane

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