benzyl 3-O-allyl-2-benzyloxycarbonylamino-2-deoxy-4,6-O-(R)-(2-methoxybenzylidene)-α-D-glucopyranoside

Base Information

Chemical Name:benzyl 3-O-allyl-2-benzyloxycarbonylamino-2-deoxy-4,6-O-(R)-(2-methoxybenzylidene)-α-D-glucopyranoside
CAS No.:195254-04-7
Molecular Formula:C₃₂H₃₅NO₈
Molecular Weight:561.632
Hs Code.:

Synonyms:benzyl 3-O-allyl-2-benzyloxycarbonylamino-2-deoxy-4,6-O-(R)-(2-methoxybenzylidene)-α-D-glucopyranoside

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Chemical Property of benzyl 3-O-allyl-2-benzyloxycarbonylamino-2-deoxy-4,6-O-(R)-(2-methoxybenzylidene)-α-D-glucopyranoside

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Technology Process of benzyl 3-O-allyl-2-benzyloxycarbonylamino-2-deoxy-4,6-O-(R)-(2-methoxybenzylidene)-α-D-glucopyranoside

There total 3 articles about benzyl 3-O-allyl-2-benzyloxycarbonylamino-2-deoxy-4,6-O-(R)-(2-methoxybenzylidene)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 106-95-6
allyl bromide

: 195254-01-4
benzyl 2-benzyloxycarbonylamino-2-deoxy-4,6-O-(R)-(2-methoxybenzylidene)-α-D-glucopyranoside

: 195254-04-7
benzyl 3-O-allyl-2-benzyloxycarbonylamino-2-deoxy-4,6-O-(R)-(2-methoxybenzylidene)-α-D-glucopyranoside

Guidance literature:: With potassium hydroxide; In 1,4-dioxane; for 16h; Heating;
DOI:10.1080/07328309708006541

Reference yield:

: 58378-33-9
o-anisaldehyde dimethyl acetal

: 195254-04-7
benzyl 3-O-allyl-2-benzyloxycarbonylamino-2-deoxy-4,6-O-(R)-(2-methoxybenzylidene)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / dimethylformamide / 3 h / 85 °C / 187.5 Torr

2: 91 percent / KOH / dioxane / 16 h / Heating

With potassium hydroxide; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1080/07328309708006541

Reference yield:

: 135-02-4
ortho-anisaldehyde

: 195254-04-7
benzyl 3-O-allyl-2-benzyloxycarbonylamino-2-deoxy-4,6-O-(R)-(2-methoxybenzylidene)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: CSA / methanol / 6 h / Ambient temperature

2: 93 percent / dimethylformamide / 3 h / 85 °C / 187.5 Torr

3: 91 percent / KOH / dioxane / 16 h / Heating

With potassium hydroxide; camphor-10-sulfonic acid; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;
DOI:10.1080/07328309708006541