C₃₂H₃₁F₂N₃O₂

Base Information

Chemical Name:C₃₂H₃₁F₂N₃O₂
CAS No.:845973-13-9
Molecular Formula:C₃₂H₃₁F₂N₃O₂
Molecular Weight:527.614
Hs Code.:

C<sub>32</sub>H<sub>31</sub>F<sub>2</sub>N<sub>3</sub>O<sub>2</sub>

Synonyms:C₃₂H₃₁F₂N₃O₂

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Chemical Property of C₃₂H₃₁F₂N₃O₂

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Technology Process of C₃₂H₃₁F₂N₃O₂

There total 7 articles about C₃₂H₃₁F₂N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 616-45-5
2-pyrrolidinon

: 845543-99-9
C₂₈H₂₅ClF₂N₂O

: 845973-13-9
C₃₂H₃₁F₂N₃O₂

Guidance literature:: With copper(l) iodide; (R,R)-N,N'-dimethyl-1,2-diaminocyclohexane; potassium carbonate; In 1,4-dioxane; at 130 ℃; for 37h; Heating;

Reference yield:

: 473567-47-4
methyl (S)-2-((tert-butoxycarbonyl)amino)-3-(3,5-difluorophenyl)propanoate

: 845973-13-9
C₃₂H₃₁F₂N₃O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride / 1,4-dioxane; methanol; dichloromethane / 4 h / 0 - 20 °C

2.1: sodium hydrogencarbonate / tetrahydrofuran; dimethyl sulfoxide / 24 h / 20 - 70 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / 0 - 20 °C

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.67 h / -78 °C

4.2: 2 h / 20 °C

5.1: n-butyllithium; 2-(N,N-dimethylamino)ethanol / hexane / 1.5 h / -78 °C

5.2: 0.5 h / -78 - 0 °C

6.1: copper(l) iodide; (R,R)-N,N'-dimethyl-1,2-diaminocyclohexane; potassium carbonate / 1,4-dioxane / 37 h / 130 °C / Heating

With hydrogenchloride; copper(l) iodide; lithium aluminium tetrahydride; n-butyllithium; 2-(N,N-dimethylamino)ethanol; oxalyl dichloride; (R,R)-N,N'-dimethyl-1,2-diaminocyclohexane; sodium hydrogencarbonate; potassium carbonate; dimethyl sulfoxide; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; dimethyl sulfoxide;

Reference yield:

: 100-39-0
benzyl bromide

: 845973-13-9
C₃₂H₃₁F₂N₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydrogencarbonate / tetrahydrofuran; dimethyl sulfoxide / 24 h / 20 - 70 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / 0 - 20 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.67 h / -78 °C

3.2: 2 h / 20 °C

4.1: n-butyllithium; 2-(N,N-dimethylamino)ethanol / hexane / 1.5 h / -78 °C

4.2: 0.5 h / -78 - 0 °C

5.1: copper(l) iodide; (R,R)-N,N'-dimethyl-1,2-diaminocyclohexane; potassium carbonate / 1,4-dioxane / 37 h / 130 °C / Heating

With copper(l) iodide; lithium aluminium tetrahydride; n-butyllithium; 2-(N,N-dimethylamino)ethanol; oxalyl dichloride; (R,R)-N,N'-dimethyl-1,2-diaminocyclohexane; sodium hydrogencarbonate; potassium carbonate; dimethyl sulfoxide; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; dimethyl sulfoxide;