(R)-3-Hydroxy-4-(4-methoxy-phenyl)-thiobutyric acid S-pyridin-2-yl ester

Base Information

Chemical Name:(R)-3-Hydroxy-4-(4-methoxy-phenyl)-thiobutyric acid S-pyridin-2-yl ester
CAS No.:153525-09-8
Molecular Formula:C₁₆H₁₇NO₃S
Molecular Weight:303.382
Hs Code.:

Synonyms:(R)-3-Hydroxy-4-(4-methoxy-phenyl)-thiobutyric acid S-pyridin-2-yl ester

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Chemical Property of (R)-3-Hydroxy-4-(4-methoxy-phenyl)-thiobutyric acid S-pyridin-2-yl ester

Chemical Property:

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Technology Process of (R)-3-Hydroxy-4-(4-methoxy-phenyl)-thiobutyric acid S-pyridin-2-yl ester

There total 5 articles about (R)-3-Hydroxy-4-(4-methoxy-phenyl)-thiobutyric acid S-pyridin-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 2127-03-9
2,2'-dipyridyldisulphide

: 153525-04-3
(R)-(-)-3-Hydroxy-4-(4-methoxyphenyl)butanoic acid

: 153525-09-8
(R)-3-Hydroxy-4-(4-methoxy-phenyl)-thiobutyric acid S-pyridin-2-yl ester

Guidance literature:: With triphenylphosphine; In chloroform; Ambient temperature;
DOI:10.1021/jo00079a049

Reference yield:

: 153525-08-7
5-[1-Hydroxy-2-(4-methoxy-phenyl)-ethylidene]-2,2-dimethyl-[1,3]dioxane-4,6-dione

: 153525-09-8
(R)-3-Hydroxy-4-(4-methoxy-phenyl)-thiobutyric acid S-pyridin-2-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 3 h / Heating

2: 96 percent / H₂ / (R)-BINAP-Ru(II) / ethanol / 80 °C / 76000 - 83600 Torr

3: 96 percent / aq. KOH / ethanol / 24 h / 0 °C

4: 95 percent / triphenylphosphine / CHCl₃ / Ambient temperature

With potassium hydroxide; hydrogen; triphenylphosphine; (R)-BINAP-Ru(II); In ethanol; chloroform;
DOI:10.1021/jo00079a049

Reference yield:

: 32711-91-4
ethyl 4-(4-methoxylphenyl)-3-oxobutanoate

: 153525-09-8
(R)-3-Hydroxy-4-(4-methoxy-phenyl)-thiobutyric acid S-pyridin-2-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / H₂ / (R)-BINAP-Ru(II) / ethanol / 80 °C / 76000 - 83600 Torr

2: 96 percent / aq. KOH / ethanol / 24 h / 0 °C

3: 95 percent / triphenylphosphine / CHCl₃ / Ambient temperature

With potassium hydroxide; hydrogen; triphenylphosphine; (R)-BINAP-Ru(II); In ethanol; chloroform;
DOI:10.1021/jo00079a049