3,4-Bis-benzyloxy-benzoic acid 2-acetyl-3,5-dimethoxy-4-octadecyloxy-phenyl ester

Base Information

• Chemical Name: 3,4-Bis-benzyloxy-benzoic acid 2-acetyl-3,5-dimethoxy-4-octadecyloxy-phenyl ester
• CAS No.: 103777-55-5
• Molecular Formula: C₄₉H₆₄O₈
• Molecular Weight: 781.042

Synonyms:3,4-Bis-benzyloxy-benzoic acid 2-acetyl-3,5-dimethoxy-4-octadecyloxy-phenyl ester

Chemical Property of 3,4-Bis-benzyloxy-benzoic acid 2-acetyl-3,5-dimethoxy-4-octadecyloxy-phenyl ester

Chemical Property:

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Technology Process of 3,4-Bis-benzyloxy-benzoic acid 2-acetyl-3,5-dimethoxy-4-octadecyloxy-phenyl ester

There total 3 articles about 3,4-Bis-benzyloxy-benzoic acid 2-acetyl-3,5-dimethoxy-4-octadecyloxy-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

n-iodooctadecane (629-93-6) → 3,4-Bis-benzyloxy-benzoic acid 2-acetyl-3,5-dimethoxy-4-octadecyloxy-phenyl ester (103777-55-5)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / acetone / Heating

2: pyridine / 3 h / 120 °C

With pyridine; potassium carbonate; In acetone;

DOI:10.1021/jm00161a021

Reference yield:

3,6-dihydroxy-2,4-dimethoxyacetophenone (6962-57-8) → 3,4-Bis-benzyloxy-benzoic acid 2-acetyl-3,5-dimethoxy-4-octadecyloxy-phenyl ester (103777-55-5)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / acetone / Heating

2: pyridine / 3 h / 120 °C

With pyridine; potassium carbonate; In acetone;

DOI:10.1021/jm00161a021

Reference yield:

3,4-dibenzyloxybenzoyl chloride (1486-54-0) + 1-(6-Hydroxy-2,4-dimethoxy-3-octadecyloxy-phenyl)-ethanone (103777-41-9) → 3,4-Bis-benzyloxy-benzoic acid 2-acetyl-3,5-dimethoxy-4-octadecyloxy-phenyl ester (103777-55-5)

Guidance literature:

With pyridine; at 120 ℃; for 3h;

DOI:10.1021/jm00161a021

upstream raw materials:

3,4-dibenzyloxybenzoyl chloride

1-(6-Hydroxy-2,4-dimethoxy-3-octadecyloxy-phenyl)-ethanone

n-iodooctadecane

3,6-dihydroxy-2,4-dimethoxyacetophenone

Downstream raw materials:

2-(3,4-Bis-benzyloxy-phenyl)-5,7-dimethoxy-6-octadecyloxy-chromen-4-one

Acetic acid 2-acetoxy-5-(5,7-dimethoxy-6-octadecyloxy-4-oxo-4H-chromen-2-yl)-phenyl ester

2-(3,4-Dihydroxy-phenyl)-5,7-dimethoxy-6-octadecyloxy-chromen-4-one

2-(3,4-Dihydroxy-phenyl)-5-hydroxy-7-methoxy-6-octadecyloxy-chromen-4-one

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