(E)-3-hexenoic acid phenyl amide

Base Information

Chemical Name:(E)-3-hexenoic acid phenyl amide
CAS No.:98857-99-9
Molecular Formula:C₁₂H₁₅NO
Molecular Weight:189.257
Hs Code.:

Synonyms:(E)-3-hexenoic acid phenyl amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-hexenoic acid phenyl amide

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Technology Process of (E)-3-hexenoic acid phenyl amide

There total 2 articles about (E)-3-hexenoic acid phenyl amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1577-18-0
(E)-3-hexenoic acid

: 62-53-3
aniline

: 98857-99-9
(E)-3-hexenoic acid phenyl amide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1021/ja710492q

Reference yield:

: 504-60-9,17410-45-6,25212-15-1,64940-84-7
penta-1,3-diene

: 103-71-9
phenyl isocyanate

: 98857-98-8
(Z)-3-hexenoic acid phenyl amide

: 98857-99-9
(E)-3-hexenoic acid phenyl amide

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; sulfuric acid; tricyclohexylphosphine; Yield given. Multistep reaction. Yields of byproduct given; 1) diethylether, 48h, -10 deg C, 2) diethylether, 20h;

Reference yield: 81.0%

: 98857-99-9
(E)-3-hexenoic acid phenyl amide

: 1016225-26-5
(R)-3-hydroxy-N-phenylhexanamide

Guidance literature:: (E)-3-hexenoic acid phenyl amide; With (TADDOL)P(indoline); bis(norbornadiene)rhodium(l)tetrafluoroborate; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In tetrahydrofuran; at 0 - 20 ℃; for 25h; Inert atmosphere;

With water; dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 2h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol101932q