(R)-3-hydroxy-N-phenylhexanamide

Base Information

Chemical Name:(R)-3-hydroxy-N-phenylhexanamide
CAS No.:1016225-26-5
Molecular Formula:C₁₂H₁₇NO₂
Molecular Weight:207.272
Hs Code.:

Synonyms:(R)-3-hydroxy-N-phenylhexanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-3-hydroxy-N-phenylhexanamide

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Technology Process of (R)-3-hydroxy-N-phenylhexanamide

There total 6 articles about (R)-3-hydroxy-N-phenylhexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 98857-98-8
(Z)-3-hexenoic acid phenyl amide

: 1016225-26-5
(R)-3-hydroxy-N-phenylhexanamide

Guidance literature:: (Z)-3-hexenoic acid phenyl amide; With (TADDOL)P(indoline); bis(norbornadiene)rhodium(l)tetrafluoroborate; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In tetrahydrofuran; at 0 - 20 ℃; for 25h; Inert atmosphere;

With water; dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 2h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol101932q

Reference yield: 81.0%

: 98857-99-9
(E)-3-hexenoic acid phenyl amide

: 1016225-26-5
(R)-3-hydroxy-N-phenylhexanamide

Guidance literature:: (E)-3-hexenoic acid phenyl amide; With (TADDOL)P(indoline); bis(norbornadiene)rhodium(l)tetrafluoroborate; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In tetrahydrofuran; at 0 - 20 ℃; for 25h; Inert atmosphere;

With water; dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 2h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol101932q

Reference yield:

: 98857-98-8
(Z)-3-hexenoic acid phenyl amide

: 1016225-26-5
(R)-3-hydroxy-N-phenylhexanamide

: 1016225-14-1
(S)-3-hydroxy-N-phenylhexanamide

Guidance literature:: (Z)-3-hexenoic acid phenyl amide; With (TADDOL)P(indoline); bis(norbornadiene)rhodium(l)tetrafluoroborate; (3,5-dimethylphenyl-TADDOL)POPh; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In tetrahydrofuran; at 0 - 20 ℃; for 25h; Inert atmosphere;

With water; dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 2h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol101932q