2-[(4-methylbenzenesulfonyl)oxy]ethyl 4-nitrophenyl methanephosphonate

Base Information

Chemical Name:2-[(4-methylbenzenesulfonyl)oxy]ethyl 4-nitrophenyl methanephosphonate
CAS No.:1428268-08-9
Molecular Formula:C₁₆H₁₈NO₈PS
Molecular Weight:415.361
Hs Code.:

Synonyms:2-[(4-methylbenzenesulfonyl)oxy]ethyl 4-nitrophenyl methanephosphonate

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Chemical Property of 2-[(4-methylbenzenesulfonyl)oxy]ethyl 4-nitrophenyl methanephosphonate

Chemical Property:

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Technology Process of 2-[(4-methylbenzenesulfonyl)oxy]ethyl 4-nitrophenyl methanephosphonate

There total 4 articles about 2-[(4-methylbenzenesulfonyl)oxy]ethyl 4-nitrophenyl methanephosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42772-85-0
2-hydroxyethyl 4-methylbenzenesulfonate

: 1832-64-0
4-nitrophenoxy hydrogen methylphosphonate

: 1428268-08-9
2-[(4-methylbenzenesulfonyl)oxy]ethyl 4-nitrophenyl methanephosphonate

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/j.bmcl.2013.02.010

Reference yield:

: 6395-57-9
O,O-di-4-nitrophenyl methylphosphonate

: 1428268-08-9
2-[(4-methylbenzenesulfonyl)oxy]ethyl 4-nitrophenyl methanephosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide / acetonitrile / 1.33 h / 20 °C

2: dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C

With dicyclohexyl-carbodiimide; lithium hydroxide; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2013.02.010

Reference yield:

: 1832-64-0
4-nitrophenoxy hydrogen methylphosphonate

: 1428268-08-9
2-[(4-methylbenzenesulfonyl)oxy]ethyl 4-nitrophenyl methanephosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C

2: acetonitrile / 4 h / 65 °C

With dicyclohexyl-carbodiimide; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2013.02.010