O-2-fluoroethyl-O-p-nitrophenyl methyphosphonothionate

Base Information

Chemical Name:O-2-fluoroethyl-O-p-nitrophenyl methyphosphonothionate
CAS No.:889-14-5
Molecular Formula:C₉H₁₁FNO₄PS
Molecular Weight:279.229
Hs Code.:

Synonyms:O-2-fluoroethyl-O-p-nitrophenyl methyphosphonothionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-2-fluoroethyl-O-p-nitrophenyl methyphosphonothionate

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Technology Process of O-2-fluoroethyl-O-p-nitrophenyl methyphosphonothionate

There total 7 articles about O-2-fluoroethyl-O-p-nitrophenyl methyphosphonothionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1428268-01-2
O-(2-fluoroethyl)-O-(p-nitrophenyl) methylphosphonate

: 889-14-5
O-2-fluoroethyl-O-p-nitrophenyl methyphosphonothionate

Guidance literature:: With Lawessons reagent; In toluene; at 80 ℃; for 3h;
DOI:10.1016/j.bmcl.2013.02.010

Reference yield: 33.0%

: 1428268-16-9
C₁₆H₁₈NO₇PS₂

: 889-14-5
O-2-fluoroethyl-O-p-nitrophenyl methyphosphonothionate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.166667h;
DOI:10.1016/j.bmcl.2013.02.010

Reference yield:

: 6395-57-9
O,O-di-4-nitrophenyl methylphosphonate

: 889-14-5
O-2-fluoroethyl-O-p-nitrophenyl methyphosphonothionate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydroxide / acetonitrile / 1.33 h / 20 °C

2: dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C

3: Lawessons reagent / toluene / 3 h / 80 °C

With Lawessons reagent; dicyclohexyl-carbodiimide; lithium hydroxide; In dichloromethane; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2013.02.010