tricyclohexylphosphine-monoiodoborane

Base Information

Chemical Name:tricyclohexylphosphine-monoiodoborane
CAS No.:153739-19-6
Molecular Formula:C₁₈H₃₅BIP
Molecular Weight:420.165
Hs Code.:

Synonyms:tricyclohexylphosphine-monoiodoborane

Suppliers and Price of tricyclohexylphosphine-monoiodoborane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tricyclohexylphosphine-monoiodoborane

Chemical Property:

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Technology Process of tricyclohexylphosphine-monoiodoborane

There total 2 articles about tricyclohexylphosphine-monoiodoborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: C₃₆H₆₆B₂I₂P₂

: 1333-74-0
hydrogen

: 153739-19-6
tricyclohexylphosphine-monoiodoborane

Guidance literature:: at 80 ℃; for 1h; Sealed tube;
DOI:10.1002/anie.201814230

Reference yield:

: 2622-14-2
tricyclohexylphosphine

: 153739-19-6
tricyclohexylphosphine-monoiodoborane

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 1.5 h / 20 °C

2: potassium graphite / benzene / 3 h / 20 °C

3: 1 h / 80 °C / Sealed tube

With potassium graphite; In benzene;
DOI:10.1002/anie.201814230

Reference yield: 66.0%

: 153739-19-6
tricyclohexylphosphine-monoiodoborane

: 616-38-6
carbonic acid dimethyl ester

: 287923-06-2
(C₆H₁₁)3PBH₂CO₂CH₃

Guidance literature:: With lithium 4,4'-di-tert-butylbiphenylide; TMEDA; In tetrahydrofuran; boron complex was reduced with 2 equiv. of Li deriv. at -78° andthen reacted with (MeO)2CO;
DOI:10.1021/ja0011764