(Z)-1-methoxy-3-(4-methoxy-2-methylbenzylidene)-1,3-dihydroisobenzofuran

Base Information

Chemical Name:(Z)-1-methoxy-3-(4-methoxy-2-methylbenzylidene)-1,3-dihydroisobenzofuran
CAS No.:1246365-04-7
Molecular Formula:C₁₈H₁₈O₃
Molecular Weight:282.339
Hs Code.:

Synonyms:(Z)-1-methoxy-3-(4-methoxy-2-methylbenzylidene)-1,3-dihydroisobenzofuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1-methoxy-3-(4-methoxy-2-methylbenzylidene)-1,3-dihydroisobenzofuran

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Technology Process of (Z)-1-methoxy-3-(4-methoxy-2-methylbenzylidene)-1,3-dihydroisobenzofuran

There total 2 articles about (Z)-1-methoxy-3-(4-methoxy-2-methylbenzylidene)-1,3-dihydroisobenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 67-56-1
methanol

: 1173882-93-3
2-[(4-methoxy-2-methylphenyl)ethynyl]benzaldehyde

: 1246365-04-7
(Z)-1-methoxy-3-(4-methoxy-2-methylbenzylidene)-1,3-dihydroisobenzofuran

Guidance literature:: With potassium tert-butylate; at 110 ℃; for 2.5h; regioselective reaction; Microwave irradiation; Sealed tube;
DOI:10.1055/s-0029-1218766

Reference yield: 79.0%

: 67-56-1
methanol

: 74331-69-4
1-ethynyl-4-methoxy-2-methylbenzene

: 6630-33-7
ortho-bromobenzaldehyde

: 1246365-04-7
(Z)-1-methoxy-3-(4-methoxy-2-methylbenzylidene)-1,3-dihydroisobenzofuran

Guidance literature:: methanol; 1-ethynyl-4-methoxy-2-methylbenzene; ortho-bromobenzaldehyde; With bis-triphenylphosphine-palladium(II) chloride; potassium tert-butylate; at 20 ℃; for 0.166667h; Inert atmosphere;

With copper(l) iodide; at 130 ℃; for 4h; Inert atmosphere; Sealed vessel; Microwave irradiation;
DOI:10.1016/j.tet.2010.12.056