Technology Process of C27H36O5
There total 15 articles about C27H36O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
camphor-10-sulfonic acid;
at 20 ℃;
for 1h;
DOI:10.1021/ol0701013
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 85 percent / boric acid; H2 / W-2 Raney nickel / H2O; methanol / 6 h / 20 °C
2: 89 percent / L-selectride / tetrahydrofuran / 1 h / cooling
3: 98 percent / camphorsulfonic acid / 1 h / 20 °C
With
camphor-10-sulfonic acid; hydrogen; boric acid; L-Selectride;
W-2 Raney nickel;
In
tetrahydrofuran; methanol; water;
DOI:10.1021/ol0701013
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1.28 g / KF / propan-2-ol / 20 °C
2: 95 percent / methanesulfochloride; triethylamine / CH2Cl2 / 0.08 h / 0 °C
3: zinc; aq. acetic acid / tetrahydrofuran / 0.08 h / 0 °C
4: 592 mg / sodium hypochlorite / H2O; CH2Cl2 / 5 h / 20 °C
5: 85 percent / boric acid; H2 / W-2 Raney nickel / H2O; methanol / 6 h / 20 °C
6: 89 percent / L-selectride / tetrahydrofuran / 1 h / cooling
7: 98 percent / camphorsulfonic acid / 1 h / 20 °C
With
potassium fluoride; sodium hypochlorite; camphor-10-sulfonic acid; hydrogen; boric acid; L-Selectride; acetic acid; triethylamine; zinc;
W-2 Raney nickel;
In
tetrahydrofuran; methanol; dichloromethane; water; isopropyl alcohol;
DOI:10.1021/ol0701013
