9-(2,6-diethyl-4-methylphenyl)-10-oxo-3-oxaspiro[5.5]undec-8-enyl 3,3-dimethylbutyrate

Base Information

Chemical Name:9-(2,6-diethyl-4-methylphenyl)-10-oxo-3-oxaspiro[5.5]undec-8-enyl 3,3-dimethylbutyrate
CAS No.:1058730-25-8
Molecular Formula:C₂₇H₃₈O₄
Molecular Weight:426.596
Hs Code.:

Synonyms:9-(2,6-diethyl-4-methylphenyl)-10-oxo-3-oxaspiro[5.5]undec-8-enyl 3,3-dimethylbutyrate

Suppliers and Price of 9-(2,6-diethyl-4-methylphenyl)-10-oxo-3-oxaspiro[5.5]undec-8-enyl 3,3-dimethylbutyrate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 9-(2,6-diethyl-4-methylphenyl)-10-oxo-3-oxaspiro[5.5]undec-8-enyl 3,3-dimethylbutyrate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 9-(2,6-diethyl-4-methylphenyl)-10-oxo-3-oxaspiro[5.5]undec-8-enyl 3,3-dimethylbutyrate

There total 8 articles about 9-(2,6-diethyl-4-methylphenyl)-10-oxo-3-oxaspiro[5.5]undec-8-enyl 3,3-dimethylbutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7065-46-5
3,3-dimethylbutanoic acid chloride

: 1068095-37-3
9-(2,6-diethyl-4-methylphenyl)-3-oxaspiro[5.5]undecane-8,10-dione

: 1058730-25-8
9-(2,6-diethyl-4-methylphenyl)-10-oxo-3-oxaspiro[5.5]undec-8-enyl 3,3-dimethylbutyrate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 1058731-63-7
1-(3,6-dihydro-2H-pyran-4-yl)propan-2-one

: 1058730-25-8
9-(2,6-diethyl-4-methylphenyl)-10-oxo-3-oxaspiro[5.5]undec-8-enyl 3,3-dimethylbutyrate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium ethanolate / ethanol / 4 h / 20 °C / Heating / reflux

2.1: sodium hydroxide; water / 20 °C

2.2: 2 h / 70 °C / pH 2 - 3

3.1: sodium carbonate / ethanol; water / 0.08 h / 20 °C

3.2: 4.17 h / 5 - 20 °C

4.1: lithium hydroxide / palladium diacetate / 1,2-dimethoxyethane; ethanol; water / 17 - 18 h / 0 - 50 °C

4.2: 0 °C / pH 2 - 3

5.1: triethylamine / dichloromethane / 20 °C

With lithium hydroxide; sodium hydroxide; water; sodium ethanolate; sodium carbonate; triethylamine; palladium diacetate; In 1,2-dimethoxyethane; ethanol; dichloromethane; water;

Reference yield:

: 29943-42-8,143562-54-3
Tetrahydro-4H-pyran-4-one

: 1058730-25-8
9-(2,6-diethyl-4-methylphenyl)-10-oxo-3-oxaspiro[5.5]undec-8-enyl 3,3-dimethylbutyrate

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium hydroxide / ethanol; water / 5 h / 5 - 20 °C

2.1: sodium ethanolate / ethanol / 4 h / 20 °C / Heating / reflux

3.1: sodium hydroxide; water / 20 °C

3.2: 2 h / 70 °C / pH 2 - 3

4.1: sodium carbonate / ethanol; water / 0.08 h / 20 °C

4.2: 4.17 h / 5 - 20 °C

5.1: lithium hydroxide / palladium diacetate / 1,2-dimethoxyethane; ethanol; water / 17 - 18 h / 0 - 50 °C

5.2: 0 °C / pH 2 - 3

6.1: triethylamine / dichloromethane / 20 °C

With potassium hydroxide; lithium hydroxide; sodium hydroxide; water; sodium ethanolate; sodium carbonate; triethylamine; palladium diacetate; In 1,2-dimethoxyethane; ethanol; dichloromethane; water;