meso-mono<α-o-(phenylcarbamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

Base Information

Chemical Name:meso-mono<α-o-(phenylcarbamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin
CAS No.:139870-27-2
Molecular Formula:C₆₆H₆₃N₉O₄
Molecular Weight:1046.28
Hs Code.:

Synonyms:meso-mono<α-o-(phenylcarbamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of meso-mono<α-o-(phenylcarbamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

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Technology Process of meso-mono<α-o-(phenylcarbamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

There total 4 articles about meso-mono<α-o-(phenylcarbamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 103-71-9
phenyl isocyanate

: 75557-89-0
meso-β-(o-aminophenyl)-α,α,α-tris<(o-pyvalamido)phenyl>porphyrin

: 139870-27-2
meso-mono<α-o-(phenylcarbamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

Guidance literature:: In dichloromethane; at 0 ℃;

Reference yield:

: 3282-30-2
pivaloyl chloride

: 139870-27-2
meso-mono<α-o-(phenylcarbamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / CH₂Cl₂ / 3 h / 0 °C

2: Cl₃CCOOH / CH₂Cl₂ / 0 °C

3: 53 percent / CH₂Cl₂ / 0 °C

With potassium carbonate; trichloroacetic acid; In dichloromethane;

Reference yield:

: 85294-22-0
meso-tris(α,α,α-o-aminophenyl)mono<α-o-<(triphenylmethyl)amino>phenyl>porphyrin

: 139870-27-2
meso-mono<α-o-(phenylcarbamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / CH₂Cl₂ / 3 h / 0 °C

2: Cl₃CCOOH / CH₂Cl₂ / 0 °C

3: 53 percent / CH₂Cl₂ / 0 °C

With potassium carbonate; trichloroacetic acid; In dichloromethane;