SALICYLIC ACID 4-NITROPHENYL ESTER

Base Information

• Chemical Name: SALICYLIC ACID 4-NITROPHENYL ESTER
• CAS No.: 17374-48-0
• Molecular Formula: C13H9 N O5
• Molecular Weight: 259.218
• Mol file: 17374-48-0.mol

Synonyms:Salicylicacid, p-nitrophenyl ester (6CI,7CI,8CI); Phenol, p-nitro-, salicylate (8CI);4-Nitrophenyl salicylate; p-Nitrophenyl salicylate

Chemical Property of SALICYLIC ACID 4-NITROPHENYL ESTER

Chemical Property:

• Melting Point: 148°C
• Boiling Point: 409.2±25.0 °C(Predicted)
• PKA: 7.32±0.30(Predicted)
• PSA: 92.35000
• Density: 1.415±0.06 g/cm3(Predicted)
• LogP: 3.04280

Purity/Quality:

98% ^*data from raw suppliers

4-Nitrophenyl Salicylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of SALICYLIC ACID 4-NITROPHENYL ESTER

There total 9 articles about SALICYLIC ACID 4-NITROPHENYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

Acetylsalicylsaeure-4-nitrophenylester (77008-82-3) → Salicylsaeure-4-nitrophenylester (17374-48-0)

Guidance literature:

With phosphate buffer; In 1,4-dioxane;

Reference yield: 47.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + 2-(trifluoromethyl)phenol (444-30-4) → Salicylsaeure-4-nitrophenylester (17374-48-0) + 2-(trifluoromethyl)phenyl 2-hydroxybenzoate + salicylic acid (69-72-7,25496-36-0,8052-31-1)

Guidance literature:

With water; potassium carbonate; In toluene; at 120 ℃; for 12h;

DOI:10.1016/j.tetlet.2021.153592

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + salicylic acid (69-72-7,25496-36-0,8052-31-1) → Salicylsaeure-4-nitrophenylester (17374-48-0)

Guidance literature:

With trichlorophosphate;

upstream raw materials:

4-nitro-phenol

salicylic acid

bis(p-nitrophenyl)sulfite

Acetylsalicylsaeure-4-nitrophenylester

Downstream raw materials:

o-carboxyphenyl p-nitrophenyl ether

salicylic acid-(4-amino-phenyl ester)

N,N'-Bis(2-hydroxybenzoyl)-1,6-diaminohexane

p-nitrophenolate

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