lithium 4-(5-(3-cyanophenyl)-1,3-dimethyl-2,4-dioxo-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)butanoate

Base Information

Chemical Name:lithium 4-(5-(3-cyanophenyl)-1,3-dimethyl-2,4-dioxo-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)butanoate
CAS No.:1614251-70-5
Molecular Formula:C₁₉H₁₇N₄O₄*Li
Molecular Weight:372.309
Hs Code.:

Synonyms:lithium 4-(5-(3-cyanophenyl)-1,3-dimethyl-2,4-dioxo-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)butanoate

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Chemical Property of lithium 4-(5-(3-cyanophenyl)-1,3-dimethyl-2,4-dioxo-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)butanoate

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Technology Process of lithium 4-(5-(3-cyanophenyl)-1,3-dimethyl-2,4-dioxo-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)butanoate

There total 7 articles about lithium 4-(5-(3-cyanophenyl)-1,3-dimethyl-2,4-dioxo-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1614251-42-1
methyl 4-(5-(3-cyanophenyl)-1,3-dimethyl-2,4-dioxo-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)butanoate

: 1614251-70-5
lithium 4-(5-(3-cyanophenyl)-1,3-dimethyl-2,4-dioxo-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)butanoate

Guidance literature:: With lithium hydroxide monohydrate; water; In tetrahydrofuran; for 2h;

Reference yield:

: 1613623-81-6
1,3-dimethyl-2,4-dioxo-6-((2-(trimethylsilyl)ethoxy)methyl)-2,3,4,6-tetrahydro-1H-pyrrolo[3,4-d]pyrimidin-5-ylboronic acid

: 1614251-70-5
lithium 4-(5-(3-cyanophenyl)-1,3-dimethyl-2,4-dioxo-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)butanoate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetic acid butyl ester; water / 1.5 h / 80 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 60 °C

3: caesium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

4: lithium hydroxide monohydrate; water / tetrahydrofuran / 2 h

With lithium hydroxide monohydrate; tetrabutyl ammonium fluoride; water; potassium carbonate; caesium carbonate; In tetrahydrofuran; acetic acid butyl ester; water; N,N-dimethyl-formamide;

Reference yield:

: 1613623-83-8
3-(1,3-dimethyl-2,4-dioxo-6-((2-(trimethylsilyl)ethoxy)methyl)-2,3,4,6-tetrahydro-1H-pyrrolo[3,4-d]pyrimidin-5-yl)benzonitrile

: 1614251-70-5
lithium 4-(5-(3-cyanophenyl)-1,3-dimethyl-2,4-dioxo-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 60 °C

2: caesium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

3: lithium hydroxide monohydrate; water / tetrahydrofuran / 2 h

With lithium hydroxide monohydrate; tetrabutyl ammonium fluoride; water; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;