N-[(3,3-dimethyloxiran-2-yl)methyl]-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

Base Information

• Chemical Name: N-[(3,3-dimethyloxiran-2-yl)methyl]-4-methyl-N-(prop-2-ynyl)benzenesulfonamide
• CAS No.: 1147121-30-9
• Molecular Formula: C₁₅H₁₉NO₃S
• Molecular Weight: 293.387

Synonyms:N-[(3,3-dimethyloxiran-2-yl)methyl]-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

Chemical Property of N-[(3,3-dimethyloxiran-2-yl)methyl]-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

Chemical Property:

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Technology Process of N-[(3,3-dimethyloxiran-2-yl)methyl]-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

There total 1 articles about N-[(3,3-dimethyloxiran-2-yl)methyl]-4-methyl-N-(prop-2-ynyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N-prenyl-N-propargyltosylamide (132330-44-0) → N-[(3,3-dimethyloxiran-2-yl)methyl]-4-methyl-N-(prop-2-ynyl)benzenesulfonamide (1147121-30-9)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2009.01.065

Reference yield: 97.0%

methanol (67-56-1) + N-[(3,3-dimethyloxiran-2-yl)methyl]-4-methyl-N-(prop-2-ynyl)benzenesulfonamide (1147121-30-9) → N-(2-hydroxy-3-methoxy-3-methylbutyl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide (1416895-61-8)

Guidance literature:

With silver trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1055/s-0031-1290466

Reference yield: 62.0%

N-[(3,3-dimethyloxiran-2-yl)methyl]-4-methyl-N-(prop-2-ynyl)benzenesulfonamide (1147121-30-9) → 6-methyl-2-(1-methylethenyl)-4-[(4-methylphenyl)-sulfonyl]-3,4-dihydro-2H-1,4-oxazine (1147121-31-0)

Guidance literature:

With platinum(II) chloride; In toluene; for 24h; Inert atmosphere; Reflux;

DOI:10.1016/j.tet.2009.01.065

upstream raw materials:

N-prenyl-N-propargyltosylamide

Downstream raw materials:

6-methyl-2-(1-methylethenyl)-4-[(4-methylphenyl)-sulfonyl]-3,4-dihydro-2H-1,4-oxazine

N-(2-hydroxy-3-methylbut-3-enyl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

4-methyl-N-(3-methyl-2-oxobutyl)-N-(prop-2-ynyl)benzenesulfonamide

2-(2-methoxypropan-2-yl)-6-methyl-4-tosyl-3,4-dihydro-2H-1,4-oxazine

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