benzyl 2-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)-2-hydroxyacetate

Base Information

Chemical Name:benzyl 2-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)-2-hydroxyacetate
CAS No.:1420039-33-3
Molecular Formula:C₂₁H₃₄O₄Si
Molecular Weight:378.584
Hs Code.:

Synonyms:benzyl 2-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)-2-hydroxyacetate

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Chemical Property of benzyl 2-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)-2-hydroxyacetate

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Technology Process of benzyl 2-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)-2-hydroxyacetate

There total 7 articles about benzyl 2-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)-2-hydroxyacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 929557-14-2
benzyl 2-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)acetate

: 1420039-33-3
benzyl 2-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)-2-hydroxyacetate

Guidance literature:: benzyl 2-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)acetate; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.833333h;

With N-(benzenesulfonyl)-3-phenyloxaziridine; In tetrahydrofuran; at -78 ℃; for 1.5h;

Reference yield:

: 929557-10-8
benzyl 2-(1,4-dioxaspiro[4,5]decan-8-yl)acetate

: 1420039-33-3
benzyl 2-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)-2-hydroxyacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / acetone; water / 15 h / 55 °C

2.1: methanol; sodium tetrahydroborate / 2 h / 0 °C

3.1: 1H-imidazole / N,N-dimethyl-formamide / 15 h / 65 °C

4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.83 h / -78 °C

4.2: 1.5 h / -78 °C

With 1H-imidazole; methanol; sodium tetrahydroborate; sodium hexamethyldisilazane; toluene-4-sulfonic acid; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 929557-11-9
benzyl 2-(4-oxocyclohexyl)acetate

: 1420039-33-3
benzyl 2-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)-2-hydroxyacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol; sodium tetrahydroborate / 2 h / 0 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 15 h / 65 °C

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.83 h / -78 °C

3.2: 1.5 h / -78 °C

With 1H-imidazole; methanol; sodium tetrahydroborate; sodium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide;