N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] heptanamide

Base Information

Chemical Name:N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] heptanamide
CAS No.:1449203-96-6
Molecular Formula:C₁₆H₂₀IN₃O₃S
Molecular Weight:461.324
Hs Code.:

Synonyms:N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] heptanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] heptanamide

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Technology Process of N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] heptanamide

There total 6 articles about N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] heptanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.55%

: C₂₃H₃₂IN₃O₄S

: 1449203-96-6
N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] heptanamide

Guidance literature:: With methanol; sodium hydroxide; for 3h; Reflux;

Reference yield:

: 5438-36-8
5-iodovaniline

: 1449203-96-6
N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] heptanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / 4 h / 20 °C

2.1: acetic acid / methanol / 6 h / pH 4 - 5 / Reflux

3.1: iron(III) chloride / methanol; water / Reflux

3.2: 1 h / Reflux

4.1: pyridine / 2 h / 20 °C

5.1: sodium hydroxide / methanol / 3 h / Reflux

With pyridine; iron(III) chloride; sulfuric acid; acetic acid; sodium hydroxide; In methanol; water;
DOI:10.1016/j.ejmech.2013.05.001

Reference yield:

: 486994-14-3
4-(acetyloxy)-3-iodo-5-methoxybenzaldehyde

: 1449203-96-6
N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] heptanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / methanol / 6 h / pH 4 - 5 / Reflux

2.1: iron(III) chloride / methanol; water / Reflux

2.2: 1 h / Reflux

3.1: pyridine / 2 h / 20 °C

4.1: sodium hydroxide / methanol / 3 h / Reflux

With pyridine; iron(III) chloride; acetic acid; sodium hydroxide; In methanol; water;
DOI:10.1016/j.ejmech.2013.05.001